1-Phenyl-pentylamine

Base Information

• Chemical Name: 1-Phenyl-pentylamine
• CAS No.: 61501-03-9
• Molecular Formula: C11H17N
• Molecular Weight: 163.263
• DSSTox Substance ID: DTXSID90475945
• Nikkaji Number: J303.697I
• Mol file: 61501-03-9.mol

Synonyms:1-PHENYL-PENTYLAMINE;1-phenylpentan-1-amine;61501-03-9;1-phenyl-pentyl-amine;SCHEMBL453579;(R)-1-Phenyl-1-pentanamine;DTXSID90475945;MFCD09251364;AKOS000169562;AKOS016037508;SY349534;CS-0297358;EN300-241680;A1-04800

Chemical Property of 1-Phenyl-pentylamine

Chemical Property:

• Vapor Pressure: 0.032mmHg at 25°C
• Refractive Index: 1.516
• Boiling Point: 243.225°C at 760 mmHg
• Flash Point: 102.027°C
• PSA: 26.02000
• Density: 0.927g/cm³
• LogP: 3.57690
• XLogP3: 2.6
• Hydrogen Bond Donor Count: 1
• Hydrogen Bond Acceptor Count: 1
• Rotatable Bond Count: 4
• Exact Mass: 163.136099547
• Heavy Atom Count: 12
• Complexity: 106

Purity/Quality:

99% ^*data from raw suppliers

1-Phenylpentan-1-amine ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CCCCC(C1=CC=CC=C1)N

Technology Process of 1-Phenyl-pentylamine

There total 35 articles about 1-Phenyl-pentylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

phenyl butyl ketone (1009-14-9) → α-n-butylbenzylamine (61501-03-9)

Guidance literature:

With nickel(II) tetrafluoroborate hexahydrate; ammonia; hydrogen; bis(2-diphenylphosphinoethyl)phenylphosphine; In 2,2,2-trifluoroethanol; at 120 ℃; for 24h; chemoselective reaction;

DOI:10.1039/d0sc01084g

Reference yield: 74.0%

tributyl borane (122-56-5) + 1-benzyl-tetrahydro-thiophenium tetrafluoroborate → α-n-butylbenzylamine (61501-03-9)

Guidance literature:

tributyl borane; 1-benzyl-tetrahydro-thiophenium tetrafluoroborate; With lithium hexamethyldisilazane; In tetrahydrofuran; 1,4-dioxane; at 5 ℃; for 5h;

With hydroxylamine-O-sulfonic acid;

DOI:10.1021/ja043632k

Reference yield: 64.0%

n-butyllithium (109-72-8,29786-93-4) + (E)-N-benzylidene-1,1,1-trimethylsilanamine (120419-97-8) → α-n-butylbenzylamine (61501-03-9)

Guidance literature:

With 2exo,3exo-dimethoxy-1,7,7-trimethyl-norbornan; In diethyl ether; hexane; at 0 ℃; for 1h;

upstream raw materials:

phenyl butyl ketone

valerophenone oxime

n-butyllithium

N-benzylidene-S-phenylthiohydroxylamine

Downstream raw materials:

3-chloro-propionic acid-(1-phenyl-pentylamide)

N-(1-Phenyl-pent-1-yl)-harnstoff

1,2-Diphenyl-2-[(E)-1-phenyl-pentylimino]-ethanone

4-Amino-N-(1-phenyl-pentyl)-benzamide