2H-Pyran-3-ol,3-ethyl-3,4-dihydro-2-phenyl-,(2R,3R)-rel-(9CI)

Base Information

Chemical Name:2H-Pyran-3-ol,3-ethyl-3,4-dihydro-2-phenyl-,(2R,3R)-rel-(9CI)
CAS No.:697300-66-6
Molecular Formula:C₁₃H₁₆O₂
Molecular Weight:204.269
Hs Code.:
Mol file:697300-66-6.mol

Synonyms:2H-Pyran-3-ol,3-ethyl-3,4-dihydro-2-phenyl-,(2R,3R)-rel-(9CI)

Suppliers and Price of 2H-Pyran-3-ol,3-ethyl-3,4-dihydro-2-phenyl-,(2R,3R)-rel-(9CI)

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2H-Pyran-3-ol,3-ethyl-3,4-dihydro-2-phenyl-,(2R,3R)-rel-(9CI)

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Technology Process of 2H-Pyran-3-ol,3-ethyl-3,4-dihydro-2-phenyl-,(2R,3R)-rel-(9CI)

There total 6 articles about 2H-Pyran-3-ol,3-ethyl-3,4-dihydro-2-phenyl-,(2R,3R)-rel-(9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 292163-77-0
rac-3-(1-allyloxphenylmethyl)penta-1,4-dien-3-ol

: 697300-66-6,796076-93-2
3-ethyl-2-phenyl-3,4-dihydro-2H-pyran-3-ol

Guidance literature:: Multi-step reaction with 2 steps

1: [Cl₂(PCy₃)2Ru=CHPh] / toluene / 20 °C

2: NaOH; 2-propanol / toluene / 110 °C

With sodium hydroxide; isopropyl alcohol; Grubbs catalyst first generation; In toluene;
DOI:10.1039/b400229f

Reference yield:

: 292163-77-0
rac-3-(1-allyloxphenylmethyl)penta-1,4-dien-3-ol

: 697300-66-6,796076-93-2
3-ethyl-2-phenyl-3,4-dihydro-2H-pyran-3-ol

: 697300-66-6,796076-93-2
3-ethyl-2-phenyl-3,4-dihydro-2H-pyran-3-ol

Guidance literature:: rac-3-(1-allyloxphenylmethyl)penta-1,4-dien-3-ol; With Grubbs catalyst first generation; In toluene; at 25 ℃;

With sodium hydroxide; Grubbs catalyst first generation; isopropyl alcohol; In toluene; at 110 ℃; for 7h; Title compound not separated from byproducts;
DOI:10.1021/jo048937w

Reference yield:

: 292163-77-0
rac-3-(1-allyloxphenylmethyl)penta-1,4-dien-3-ol

: 697300-66-6,796076-93-2
3-ethyl-2-phenyl-3,4-dihydro-2H-pyran-3-ol

: 697300-66-6,796076-93-2
3-ethyl-2-phenyl-3,4-dihydro-2H-pyran-3-ol

Guidance literature:: rac-3-(1-allyloxphenylmethyl)penta-1,4-dien-3-ol; With Grubbs catalyst first generation; In toluene; at 25 ℃;

With sodium hydroxide; Grubbs catalyst first generation; isopropyl alcohol; In toluene; at 110 ℃; for 7h; Title compound not separated from byproducts;
DOI:10.1021/jo048937w