{(E)-[1-(1-hydroxypyridin-2(1H)-ylidene)ethyl]diazenyl}(pyrrolidin-1-yl)methanethione

Base Information

Chemical Name:{(E)-[1-(1-hydroxypyridin-2(1H)-ylidene)ethyl]diazenyl}(pyrrolidin-1-yl)methanethione
CAS No.:87587-02-8
Molecular Formula:C₁₂H₁₆N₄OS
Molecular Weight:264.351
Hs Code.:

Synonyms:1-Pyrrolidinecarbothioicacid, [1-(1-oxido-2-pyridinyl)ethylidene]hydrazide (9CI);1-Pyrrolidinecarbothioic acid, [1-(2-pyridinyl)ethylidene]hydrazide, N-oxide;NSC 351079

Suppliers and Price of {(E)-[1-(1-hydroxypyridin-2(1H)-ylidene)ethyl]diazenyl}(pyrrolidin-1-yl)methanethione

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 3 raw suppliers

Chemical Property of {(E)-[1-(1-hydroxypyridin-2(1H)-ylidene)ethyl]diazenyl}(pyrrolidin-1-yl)methanethione

Chemical Property:

Vapor Pressure:2.38E-07mmHg at 25°C
Boiling Point:380.4°C at 760 mmHg
Flash Point:183.9°C
Density:1.29g/cm³

Purity/Quality:: 85.0-99.8% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of {(E)-[1-(1-hydroxypyridin-2(1H)-ylidene)ethyl]diazenyl}(pyrrolidin-1-yl)methanethione

There total 2 articles about {(E)-[1-(1-hydroxypyridin-2(1H)-ylidene)ethyl]diazenyl}(pyrrolidin-1-yl)methanethione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 123-75-1
pyrrolidine

: 87587-00-6
methyl 3-<1-(2-pyridinyl 1-oxide)ethylidene>hydrazinecarbodithioate

: 87587-02-8
Pyrrolidine-1-carbothioic acid [1-(1-oxy-pyridin-2-yl)-eth-(E)-ylidene]-hydrazide

Guidance literature:: In methanol; for 6h; Heating;
DOI:10.1021/jm00367a019

Reference yield:

: 2457-50-3
2-acetylpyridine N-oxide

: 87587-02-8
Pyrrolidine-1-carbothioic acid [1-(1-oxy-pyridin-2-yl)-eth-(E)-ylidene]-hydrazide

Guidance literature:: Multi-step reaction with 2 steps

1: 78 percent / methanol / 0.5 h / 50 °C

2: 91 percent / methanol / 6 h / Heating

In methanol;
DOI:10.1021/jm00367a019