Carbamic acid, 6-2-(acetylamino)-2-deoxy-.beta.-D-glucopyranosyloxyhexyl-, phenylmethyl ester

Base Information

Chemical Name:Carbamic acid, 6-2-(acetylamino)-2-deoxy-.beta.-D-glucopyranosyloxyhexyl-, phenylmethyl ester
CAS No.:62205-57-6
Molecular Formula:C22H34N2O8
Molecular Weight:454.521
Hs Code.:

Synonyms:Carbamic acid, 6-2-(acetylamino)-2-deoxy-.beta.-D-glucopyranosyloxyhexyl-, phenylmethyl ester

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Carbamic acid, 6-2-(acetylamino)-2-deoxy-.beta.-D-glucopyranosyloxyhexyl-, phenylmethyl ester

Chemical Property:

PSA：146.58000
LogP:1.21530

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of Carbamic acid, 6-2-(acetylamino)-2-deoxy-.beta.-D-glucopyranosyloxyhexyl-, phenylmethyl ester

There total 7 articles about Carbamic acid, 6-2-(acetylamino)-2-deoxy-.beta.-D-glucopyranosyloxyhexyl-, phenylmethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 62205-56-5,159173-77-0
6-(N-benzyloxycarbonylamino)hexyl-O-(2-acetamido-3,4,6-tri-O-acetyl-2-deoxy)-β-D-glucopyranoside

: 62205-57-6
6-[(N-Benzyloxycarbonyl)amino]hexyl 2-N-acetamido-2-deoxy-β-D-glucopyranoside

Guidance literature:: With sodium methylate; In methanol; for 24h;
DOI:10.1016/S0008-6215(00)85520-2

Reference yield:

: 17996-12-2
N-benzyloxycarbonyl-6-amino-1-hexanol

: 62205-57-6
6-[(N-Benzyloxycarbonyl)amino]hexyl 2-N-acetamido-2-deoxy-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 79 percent / trimethylsilyl trifluoromethanesulfonate; molecular sieves 4 Angstroem / CH₂Cl₂ / 40 h / 20 °C

2: NaOMe / methanol / 15 h / 20 °C

With trimethylsilyl trifluoromethanesulfonate; 4 A molecular sieve; sodium methylate; In methanol; dichloromethane;
DOI:10.1016/j.bmc.2005.02.009

Reference yield:

: 2-methyl-(3,4,6-tri-O-acetyl-1,2-dideoxy-α-D-glucopyrano)-<2,1-d>-2-oxazoline

: 62205-57-6
6-[(N-Benzyloxycarbonyl)amino]hexyl 2-N-acetamido-2-deoxy-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 79 percent / trimethylsilyl trifluoromethanesulfonate; molecular sieves 4 Angstroem / CH₂Cl₂ / 40 h / 20 °C

2: NaOMe / methanol / 15 h / 20 °C

With trimethylsilyl trifluoromethanesulfonate; 4 A molecular sieve; sodium methylate; In methanol; dichloromethane;
DOI:10.1016/j.bmc.2005.02.009