Carbamic acid, 6-2-(acetylamino)-2-deoxy-4,6-O-(1-methylethylidene)-.beta.-D-glucopyranosyloxyhexyl-, phenylmethyl ester

Base Information

Chemical Name:Carbamic acid, 6-2-(acetylamino)-2-deoxy-4,6-O-(1-methylethylidene)-.beta.-D-glucopyranosyloxyhexyl-, phenylmethyl ester
CAS No.:74653-29-5
Molecular Formula:C25H38 N2 O8
Molecular Weight:494.58
Hs Code.:

Synonyms:Pyrano[3,2-d]-1,3-dioxin,carbamic acid deriv.

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Chemical Property of Carbamic acid, 6-2-(acetylamino)-2-deoxy-4,6-O-(1-methylethylidene)-.beta.-D-glucopyranosyloxyhexyl-, phenylmethyl ester

Chemical Property:

PSA：124.58000
LogP:3.01360

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of Carbamic acid, 6-2-(acetylamino)-2-deoxy-4,6-O-(1-methylethylidene)-.beta.-D-glucopyranosyloxyhexyl-, phenylmethyl ester

There total 4 articles about Carbamic acid, 6-2-(acetylamino)-2-deoxy-4,6-O-(1-methylethylidene)-.beta.-D-glucopyranosyloxyhexyl-, phenylmethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 62205-57-6
6-[(N-Benzyloxycarbonyl)amino]hexyl 2-N-acetamido-2-deoxy-β-D-glucopyranoside

: 77-76-9
2,2-dimethoxy-propane

: 74653-29-5
6-(benzyloxycarbonylamino)-1-hexyl 2-acetamido-2-deoxy-4,6-O-isopropylidene-β-D-glucopyranoside

Guidance literature:: With toluene-4-sulfonic acid; In N,N-dimethyl-formamide; for 12h; Ambient temperature;
DOI:10.1016/S0008-6215(00)85520-2

Reference yield:

: 62205-56-5,159173-77-0
6-(N-benzyloxycarbonylamino)hexyl-O-(2-acetamido-3,4,6-tri-O-acetyl-2-deoxy)-β-D-glucopyranoside

: 74653-29-5
6-(benzyloxycarbonylamino)-1-hexyl 2-acetamido-2-deoxy-4,6-O-isopropylidene-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 88 percent / sodium methoxide / methanol / 24 h

2: 96 percent / p-toluenesulfonic acid / dimethylformamide / 12 h / Ambient temperature

With sodium methylate; toluene-4-sulfonic acid; In methanol; N,N-dimethyl-formamide;
DOI:10.1016/S0008-6215(00)85520-2

Reference yield:

: 17996-12-2
N-benzyloxycarbonyl-6-amino-1-hexanol

: 74653-29-5
6-(benzyloxycarbonylamino)-1-hexyl 2-acetamido-2-deoxy-4,6-O-isopropylidene-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: 80 percent / mercuric cyanide / benzene; nitromethane / 72 h / Ambient temperature

2: 88 percent / sodium methoxide / methanol / 24 h

3: 96 percent / p-toluenesulfonic acid / dimethylformamide / 12 h / Ambient temperature

With sodium methylate; mercury(II) cyanide; toluene-4-sulfonic acid; In methanol; nitromethane; N,N-dimethyl-formamide; benzene;
DOI:10.1016/S0008-6215(00)85520-2