Dimethylphenylsilanol sodium salt, 97%

Base Information

• Chemical Name: Dimethylphenylsilanol sodium salt, 97%
• CAS No.: 7646-75-5
• Molecular Formula: C8H11NaOSi
• Molecular Weight: 174.25
• Mol file: 7646-75-5.mol

Synonyms:Dimethylphenylsilanol sodium salt, 97%

Chemical Property of Dimethylphenylsilanol sodium salt, 97%

Chemical Property:

• PSA: 23.06000
• LogP: 1.52920

Purity/Quality:

98%,99%, ^*data from raw suppliers

Sodium(Phenyl)dimethylsilanolate ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Dimethylphenylsilanol sodium salt, 97%

There total 4 articles about Dimethylphenylsilanol sodium salt, 97% which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

dimethyl(ethoxy)phenylsilane (1825-58-7) → sodium phenyldimethylsilanolate (7646-75-5)

Guidance literature:

With sodium hydroxide; In 1,2-dimethoxyethane; at 50 ℃;

DOI:10.1007/s11172-014-0802-5

Reference yield: 67.0%

dimethylphenylsilanol (5272-18-4) → sodium phenyldimethylsilanolate (7646-75-5)

Guidance literature:

With sodium; In diethyl ether; for 10h; Ambient temperature;

DOI:10.1016/S0022-328X(96)06898-2

Reference yield:

1,1,3,3-tetramethyl-1,3-diphenyldisiloxane (56-33-7) → sodium phenyldimethylsilanolate (7646-75-5)

Guidance literature:

With NaOH; In methanol; isopropyl alcohol;

DOI:10.1021/ja01118a042

upstream raw materials:

dimethylphenylsilanol

phenyldimethylsilyl chloride

1,1,3,3-tetramethyl-1,3-diphenyldisiloxane

dimethyl(ethoxy)phenylsilane

Downstream raw materials:

3-(dimethyl-phenyl-silanyloxy)-1,1,5,5-tetramethyl-1,3,5-triphenyl-trisiloxane

pentamethyl(phenyl)disiloxane

1,1,5,5-tetramethyl-1,3,3,5-tetraphenyl-trisiloxane

dimethylphenylsilanol

Refernces

• 1、 Cavanaugh, Marisa DiBiase,Tetrick, Stephen M.,Masi, Christopher J.,Cutler, Alan R.. "Preparation and characterization of the rhenium silyl esters (η5-C5Me5)(CO)(NO)ReC(O)OSiR3 (SiR3 = SiMe2Ph, SiEt3)". . p. 41 - 48. Retrieved 2007/10/03.