1H-Pyrazolo[3,4-b]pyridine-3-diazonium tetrafluoroborate

Base Information

Chemical Name:1H-Pyrazolo[3,4-b]pyridine-3-diazonium tetrafluoroborate
CAS No.:63682-46-2
Molecular Formula:C6H4BF3N5
Molecular Weight:0
Hs Code.:
DSSTox Substance ID:DTXSID50499127

Synonyms:63682-46-2;1H-Pyrazolo[3,4-b]pyridine-3-diazonium Tetrafluoroborate(1-);1H-Pyrazolo[3,4-b]pyridine-3-diazonium tetrafluoroborate;1H-pyrazolo[3,4-b]pyridine-3-diazonium;tetrafluoroborate;tetrafluoroboranuide;DTXSID50499127;FT-0674167;pyrazolo[3,4-b]pyridine-3-diazonium tetrafluoroborate

Suppliers and Price of 1H-Pyrazolo[3,4-b]pyridine-3-diazonium tetrafluoroborate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

TRC
1H-Pyrazolo[3,4-b]pyridine-3-diazoniumTetrafluoroborate(1-)
5g
$ 1320.00

American Custom Chemicals Corporation
1H-PYRAZOLO(3,4-B)PYRIDINE-3-DIAZONIUM TETRAFLUOROBORATE 95.00%
5G
$ 1904.70

Total 4 raw suppliers

Chemical Property of 1H-Pyrazolo[3,4-b]pyridine-3-diazonium tetrafluoroborate

Chemical Property:

PSA：69.72000
LogP:2.74248
Solubility.:DMSO
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:8
Rotatable Bond Count:0
Exact Mass:233.0495880
Heavy Atom Count:16
Complexity:214

Purity/Quality:

99% ^*data from raw suppliers

1H-Pyrazolo[3,4-b]pyridine-3-diazoniumTetrafluoroborate(1-) ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:[B-](F)(F)(F)F.C1=CC2=C(NN=C2[N+]#N)N=C1
Uses 1H-Pyrazolo[3,4-b]pyridine-3-diazonium Tetrafluoroborate(1-) (cas# 63682-46-2) is a compound useful in organic synthesis.

Technology Process of 1H-Pyrazolo[3,4-b]pyridine-3-diazonium tetrafluoroborate

There total 2 articles about 1H-Pyrazolo[3,4-b]pyridine-3-diazonium tetrafluoroborate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 6752-16-5
1H-pyrazolo[3,4-b]pyridin-3-amine

: 63682-46-2
C₆H₄N₅⁽¹⁺⁾*BF₄^(1-)

Guidance literature:: With tetrafluoroboric acid; 1-nitroisobutane; In methanol; at 0 - 5 ℃;
DOI:10.1016/j.ejmech.2013.07.046

Reference yield:

: 6602-54-6
2-chloro-3-pyridinecarbonitrile

: 63682-46-2
C₆H₄N₅⁽¹⁺⁾*BF₄^(1-)

Guidance literature:: Multi-step reaction with 2 steps

1: hydrazine / ethanol / Reflux

2: 1-nitroisobutane; tetrafluoroboric acid / methanol / 0 - 5 °C

With tetrafluoroboric acid; 1-nitroisobutane; hydrazine; In methanol; ethanol;
DOI:10.1016/j.ejmech.2013.07.046

Reference yield:

: 63682-46-2
C₆H₄N₅⁽¹⁺⁾*BF₄^(1-)

: 1470408-00-4
3-(1-(tert-butyloxycarbonyl)-1H-indol-3-yl)-1-phenyl-4-(1-(3-morpholinopropyl)-1H-pyrazolo[3,4-b]pyridine-3-yl)-1H-pyrrole-2,5-dione

Guidance literature:: Multi-step reaction with 5 steps

1: phosphinic acid / water / 20 °C

2: iodine; potassium hydroxide / N,N-dimethyl-formamide / 20 °C

3: ethylmagnesium bromide / tetrahydrofuran / -5 - 0 °C

4: lithium chloride; bis(triphenylphosphine)palladium(II) chloride / toluene / 10 h / 100 °C / Inert atmosphere

5: potassium carbonate / N,N-dimethyl-formamide / 10 h / 60 °C

With phosphinic acid; bis(triphenylphosphine)palladium(II) chloride; ethylmagnesium bromide; iodine; potassium carbonate; lithium chloride; potassium hydroxide; In tetrahydrofuran; water; N,N-dimethyl-formamide; toluene;
DOI:10.1016/j.ejmech.2013.07.046