2-Iodobiphenyl

Base Information

Chemical Name:2-Iodobiphenyl
CAS No.:64420-96-8
Molecular Formula:C12H4 D5 I
Molecular Weight:285.068
Hs Code.:
Mol file:64420-96-8.mol

Synonyms:Pentadeuterophenyl-o-jodphenyl;2-Iodobiphenyl;2-iodo-2’,3’,4’,5’,6’-d5-1,1’-biphenyl;

Suppliers and Price of 2-Iodobiphenyl

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 5 raw suppliers

Chemical Property of 2-Iodobiphenyl

Chemical Property:

PSA：0.00000
LogP:3.95820

Purity/Quality:: 98%,99%, ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 2-Iodobiphenyl

There total 1 articles about 2-Iodobiphenyl which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 215527-70-1
2,3,4,5,6-pentadeuteriumbenzeneboronic acid

: 64420-96-8
2-iodo-2’,3’,4’,5’,6’-d₅-1,1’-biphenyl

Guidance literature:: Multi-step reaction with 2 steps

1.1: potassium carbonate; palladium diacetate / acetone; water / 65 °C / Sealed tube; Inert atmosphere

2.1: hydrogenchloride; sodium nitrite / water / 1 h / Cooling

2.2: 20 °C

With hydrogenchloride; palladium diacetate; potassium carbonate; sodium nitrite; In water; acetone;
DOI:10.1021/acs.orglett.6b01300

Reference yield: 21.0%

: 64420-96-8
2-iodo-2’,3’,4’,5’,6’-d₅-1,1’-biphenyl

: C₁₅H₁₁O₂^(1-)*Cs⁽¹⁺⁾

: C₂₇H₁₃⁽²⁾H₅O₂

Guidance literature:: With palladium diacetate; sodium carbonate; In N,N-dimethyl-formamide; at 100 ℃;
DOI:10.1039/d0cc07133a

Reference yield:

: 64420-96-8
2-iodo-2’,3’,4’,5’,6’-d₅-1,1’-biphenyl

: 74-95-3
1,1-dibromomethane

: 86-73-7
9H-fluorene

: 1190085-22-3
C₁₃H₆⁽²⁾H₄

Guidance literature:: With potassium acetate; palladium diacetate; potassium hydrogencarbonate; isopropyl alcohol; In N,N-dimethyl acetamide; water; N,N-dimethyl-formamide; at 75 ℃; for 10h; Time; Overall yield = 68 %; Schlenk technique; Inert atmosphere;
DOI:10.1021/acs.orglett.6b01300