Benzeneacetic acid, -alpha--methyl-4-(3-methylbutyl)- (9CI)

Base Information

Chemical Name:Benzeneacetic acid, -alpha--methyl-4-(3-methylbutyl)- (9CI)
CAS No.:64451-77-0
Molecular Formula:C₁₄H₂₀O₂
Molecular Weight:220.312
Hs Code.:

Synonyms:Hydratropicacid, p-isopentyl- (7CI); 2-(p-Isopentylphenyl)propionic acid; L 128325

Suppliers and Price of Benzeneacetic acid, -alpha--methyl-4-(3-methylbutyl)- (9CI)

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 4 raw suppliers

Chemical Property of Benzeneacetic acid, -alpha--methyl-4-(3-methylbutyl)- (9CI)

Chemical Property:

Boiling Point:125-128 °C(Press: 0.1 Torr)
PKA:4.43±0.10(Predicted)
PSA：37.30000
Density:1.015±0.06 g/cm3(Predicted)
LogP:3.46330

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of Benzeneacetic acid, -alpha--methyl-4-(3-methylbutyl)- (9CI)

There total 6 articles about Benzeneacetic acid, -alpha--methyl-4-(3-methylbutyl)- (9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 73318-89-5,95833-51-5,95833-52-6
α-(p-prenylphenyl)propionic acid

: 64451-77-0
2-<(4-(3-methylbutyl)phenyl)>propionic acid

Guidance literature:: With sodium hydroxide; palladium on activated charcoal; hydrogen; Ambient temperature;
DOI:10.1248/cpb.34.4653

Reference yield:

: 23853-76-1
1-chloro-4-(3-methylbut-2-en-1-yl)benzene

: 64451-77-0
2-<(4-(3-methylbutyl)phenyl)>propionic acid

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) magnesium, 1,2-dibromoethane, iodine; 2.) NiCl₂ / 1.) THF, 100-110 deg C, 2 h; 2.) THF r.t., 4.5 h

2: 93 percent / NaOH / ethanol; H₂O / 6 h / Ambient temperature

3: 91 percent / 5percent Pd/C, 0.5N NaOH, hydrogen / Ambient temperature

With sodium hydroxide; palladium on activated charcoal; hydrogen; iodine; magnesium; ethylene dibromide; nickel dichloride; In ethanol; water;
DOI:10.1248/cpb.34.4653

Reference yield:

: 85475-56-5
ethyl 2-<(4-(3-methyl-2-butenyl)phenyl)>propionate

: 64451-77-0
2-<(4-(3-methylbutyl)phenyl)>propionic acid

Guidance literature:: Multi-step reaction with 2 steps

1: 93 percent / NaOH / ethanol; H₂O / 6 h / Ambient temperature

2: 91 percent / 5percent Pd/C, 0.5N NaOH, hydrogen / Ambient temperature

With sodium hydroxide; palladium on activated charcoal; hydrogen; In ethanol; water;
DOI:10.1248/cpb.34.4653