(2,6-Dichlorophenyl)methyl acetate

Base Information

Chemical Name:(2,6-Dichlorophenyl)methyl acetate
CAS No.:71172-54-8
Molecular Formula:C9H8 Cl2 O2
Molecular Weight:219.067
Hs Code.:
NSC Number:93916
DSSTox Substance ID:DTXSID10294059
Wikidata:Q82033119

Synonyms:(2,6-dichlorophenyl)methyl acetate;71172-54-8;NSC 93916;NSC93916;SCHEMBL1092493;DTXSID10294059;NSC-93916;Acetic acid 2,6-dichloro-benzyl Ester;Acetic acid, (2,6-dichlorophenyl)metyl ester

Suppliers and Price of (2,6-Dichlorophenyl)methyl acetate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 5 raw suppliers

Chemical Property of (2,6-Dichlorophenyl)methyl acetate

Chemical Property:

Vapor Pressure:0.00735mmHg at 25°C
Boiling Point:269.2°C at 760 mmHg
Flash Point:109.7°C
Density:1.318g/cm³
XLogP3:2.9
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:3
Exact Mass:217.9901349
Heavy Atom Count:13
Complexity:175

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC(=O)OCC1=C(C=CC=C1Cl)Cl

Technology Process of (2,6-Dichlorophenyl)methyl acetate

There total 1 articles about (2,6-Dichlorophenyl)methyl acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 15258-73-8
2,6-dichlorobenzyl alcohol

: 108-24-7
acetic anhydride

: 71172-54-8
acetic acid 2,6-dichloro-benzyl ester

Guidance literature:: With dmap; triethylamine; In dichloromethane; at 5 - 20 ℃;

Reference yield: 63.0%

: 71172-54-8
acetic acid 2,6-dichloro-benzyl ester

: 73183-34-3
bis(pinacol)diborane

: 956320-63-1
acetic acid 2,6-dichloro-4-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)-benzyl ester

Guidance literature:: [2,2]bipyridinyl; bis(1,5-cyclooctadiene)diiridium(I) dichloride; In n-heptane; for 19h; Heating / reflux;

Reference yield:

: 71172-54-8
acetic acid 2,6-dichloro-benzyl ester

: (R)-3-[3,5-dichloro-4'-(4-trifluoromethyl-piperidine-1-carbonyl)-biphenyl-4-ylmethyl]-1-(4-hydroxy-piperidin-1-yl)-pyrrolidin-2-one

Guidance literature:: Multi-step reaction with 8 steps

1.1: [2,2]bipyridinyl; bis(1,5-cyclooctadiene)diiridium(I) dichloride / n-heptane / 19 h / Heating / reflux

2.1: potassium carbonate / palladium diacetate; triphenylphosphine / methanol; 1,2-dimethoxyethane; water / 20 - 80 °C

3.1: methanol; water; potassium carbonate / 5 h / 20 - 33 °C

4.1: carbon tetrabromide; triphenylphosphine / dichloromethane / 0 °C

5.1: chloro-trimethyl-silane; N,N-dimethyl-ethanamine / tetrahydrofuran / 1.5 h / -10 °C

5.2: -78 - 20 °C

6.1: sodium hydroxide; water / tetrahydrofuran / 1 h / 20 °C

6.2: 1 h

7.1: acetonitrile / 1 h / 50 °C

8.1: sodium tris(acetoxy)borohydride / acetonitrile / 20 °C

With methanol; sodium hydroxide; chloro-trimethyl-silane; N,N-dimethyl-ethanamine; carbon tetrabromide; water; sodium tris(acetoxy)borohydride; potassium carbonate; triphenylphosphine; [2,2]bipyridinyl; palladium diacetate; bis(1,5-cyclooctadiene)diiridium(I) dichloride; triphenylphosphine; In tetrahydrofuran; methanol; 1,2-dimethoxyethane; n-heptane; dichloromethane; water; acetonitrile;