beta-D-arabino-Hexopyranoside, methyl 3-((((2-chloroethyl)nitrosoamino)carbonyl)amino)-2,3-dideoxy-

Base Information

Chemical Name:beta-D-arabino-Hexopyranoside, methyl 3-((((2-chloroethyl)nitrosoamino)carbonyl)amino)-2,3-dideoxy-
CAS No.:116724-62-0
Molecular Formula:C₁₀H₁₈ClN₃O₆
Molecular Weight:311.722
Hs Code.:
DSSTox Substance ID:DTXSID20151482
Wikidata:Q83017944
ChEMBL ID:CHEMBL2114134

Synonyms:BRN 6487759;beta-D-arabino-Hexopyranoside, methyl 3-((((2-chloroethyl)nitrosoamino)carbonyl)amino)-2,3-dideoxy-;116724-62-0;C10-H18-Cl-N3-O6;CHEMBL2114134;DTXSID20151482;LS-75655

Suppliers and Price of beta-D-arabino-Hexopyranoside, methyl 3-((((2-chloroethyl)nitrosoamino)carbonyl)amino)-2,3-dideoxy-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Chemical Property of beta-D-arabino-Hexopyranoside, methyl 3-((((2-chloroethyl)nitrosoamino)carbonyl)amino)-2,3-dideoxy-

Chemical Property:

Density:1.59g/cm³
XLogP3:0.9
Hydrogen Bond Donor Count:3
Hydrogen Bond Acceptor Count:7
Rotatable Bond Count:5
Exact Mass:311.0884130
Heavy Atom Count:20
Complexity:334

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:COC1CC(C(C(O1)CO)O)NC(=O)N(CCCl)N=O
Isomeric SMILES:CO[C@H]1C[C@H]([C@@H]([C@H](O1)CO)O)NC(=O)N(CCCl)N=O

Technology Process of beta-D-arabino-Hexopyranoside, methyl 3-((((2-chloroethyl)nitrosoamino)carbonyl)amino)-2,3-dideoxy-

There total 6 articles about beta-D-arabino-Hexopyranoside, methyl 3-((((2-chloroethyl)nitrosoamino)carbonyl)amino)-2,3-dideoxy- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 6386-19-2
methyl 3-azido-4,6-O-benzylidene-2,3-dideoxy-α-D-arabino-hexopyranoside

: 116724-62-0
C₁₀H₁₈ClN₃O₆

Guidance literature:: Multi-step reaction with 6 steps

1: 98 percent / acetyl chloride, methanol / Ambient temperature

2: 1) p-toluenesulfonic acid, 2) pyridine / 1) methanol, r.t., 48 h, 2) 6 h

3: 2.2 g / 1 M sodium methoxide / methanol / 4 h

4: 90 percent / Et₃N, H₂ / 10percent Pd/C / ethanol

5: dimethylformamide / 5 h / 0 °C

6: sodium nitrite / formic acid / 0.5 h

With pyridine; methanol; hydrogen; sodium methylate; toluene-4-sulfonic acid; triethylamine; acetyl chloride; sodium nitrite; palladium on activated charcoal; In methanol; formic acid; ethanol; N,N-dimethyl-formamide;
DOI:10.1021/jm00121a005

Reference yield:

: 116724-59-5
methyl 3-azido-2,3-dideoxy-β-D-arabino-hexopyranoside

: 116724-62-0
C₁₀H₁₈ClN₃O₆

Guidance literature:: Multi-step reaction with 3 steps

1: 90 percent / Et₃N, H₂ / 10percent Pd/C / ethanol

2: dimethylformamide / 5 h / 0 °C

3: sodium nitrite / formic acid / 0.5 h

With hydrogen; triethylamine; sodium nitrite; palladium on activated charcoal; In formic acid; ethanol; N,N-dimethyl-formamide;
DOI:10.1021/jm00121a005

Reference yield:

: 20379-53-7
methyl 3-azido-2,3-dideoxy-α-D-arabino-hexopyranoside

: 116724-62-0
C₁₀H₁₈ClN₃O₆

Guidance literature:: Multi-step reaction with 5 steps

1: 1) p-toluenesulfonic acid, 2) pyridine / 1) methanol, r.t., 48 h, 2) 6 h

2: 2.2 g / 1 M sodium methoxide / methanol / 4 h

3: 90 percent / Et₃N, H₂ / 10percent Pd/C / ethanol

4: dimethylformamide / 5 h / 0 °C

5: sodium nitrite / formic acid / 0.5 h

With pyridine; hydrogen; sodium methylate; toluene-4-sulfonic acid; triethylamine; sodium nitrite; palladium on activated charcoal; In methanol; formic acid; ethanol; N,N-dimethyl-formamide;
DOI:10.1021/jm00121a005