(R)-5-Benzyloxy-1,1-dimethoxyhexane

Base Information Edit

Chemical Name:(R)-5-Benzyloxy-1,1-dimethoxyhexane
CAS No.:148840-72-6
Molecular Formula:C₁₅H₂₄O₃
Molecular Weight:252.354
Hs Code.:
Mol file:148840-72-6.mol

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (R)-5-Benzyloxy-1,1-dimethoxyhexane Edit

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Technology Process of (R)-5-Benzyloxy-1,1-dimethoxyhexane

There total 2 articles about (R)-5-Benzyloxy-1,1-dimethoxyhexane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 36255-44-4
3-bromopropanal dimethyl acetal

: 148840-72-6
(R)-5-Benzyloxy-1,1-dimethoxyhexane

Guidance literature:: Multi-step reaction with 2 steps

1: 1) Mg, 1,2-dibromoethane, 2) CuCN / 1) THF, 30 min, 10 deg C, 2) THF, -20 to 25 deg C

2: 1) NaH / 1) DMF, a) 5 to 20 deg C, 1 h, b) 20 deg C, 30 min, 2) 5-15 deg C, 30 min

With sodium hydride; magnesium; ethylene dibromide;
DOI:10.1055/s-1993-25874

Reference yield:

: 100-39-0
benzyl bromide

: 148966-73-8
(R)-6,6-Dimethoxyhexan-2-ol

: 148840-72-6
(R)-5-Benzyloxy-1,1-dimethoxyhexane

Guidance literature:: With sodium hydride; Yield given. Multistep reaction; 1) DMF, a) 5 to 20 deg C, 1 h, b) 20 deg C, 30 min, 2) 5-15 deg C, 30 min;
DOI:10.1055/s-1993-25874