Mo(N₂)2((C₆H₅)2PCH₂CH₂P(C₆H₅)CH₂CH₂P(C₆H₅)2)(P(C₆H₅)3)*0.5OC₄H₈

Base Information

Chemical Name:Mo(N₂)2((C₆H₅)2PCH₂CH₂P(C₆H₅)CH₂CH₂P(C₆H₅)2)(P(C₆H₅)3)*0.5OC₄H₈
CAS No.:75420-24-5
Molecular Formula:0C₄H₈O*C₅₂H₄₈MoN₄P₄
Molecular Weight:984.868
Hs Code.:

Mo(N<sub>2</sub>)2((C<sub>6</sub>H<sub>5</sub>)2PCH<sub>2</sub>CH<sub>2</sub>P(C<sub>6</sub>H<sub>5</sub>)CH<sub>2</sub>CH<sub>2</sub>P(C<sub>6</sub>H<sub>5</sub>)2)(P(C<sub>6</sub>H<sub>5</sub>)3)*0.5OC<sub>4</sub>H<sub>8</sub>

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Chemical Property of Mo(N₂)2((C₆H₅)2PCH₂CH₂P(C₆H₅)CH₂CH₂P(C₆H₅)2)(P(C₆H₅)3)*0.5OC₄H₈

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Technology Process of Mo(N₂)2((C₆H₅)2PCH₂CH₂P(C₆H₅)CH₂CH₂P(C₆H₅)2)(P(C₆H₅)3)*0.5OC₄H₈

There total 5 articles about Mo(N₂)2((C₆H₅)2PCH₂CH₂P(C₆H₅)CH₂CH₂P(C₆H₅)2)(P(C₆H₅)3)*0.5OC₄H₈ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 89709-79-5
{MoCl₂(C₆H₅P(CH₂CH₂P(C₆H₅)2)2)(P(C₆H₅)3)}

: 74707-26-9,75420-24-5
trans-[Mo(N₂)(PhP(CH₂CH₂PPh₂)2)(PPh₃)]

Guidance literature:: With Na/Hg; triphenylphosphine; N₂; In tetrahydrofuran; addn. of Mo complex to sodium amalgam (excess), PPh3 and THF; stirring under N2 at room temp. for 20 h;; filtration; addn. of CH3OH to the filtrate and cooling to 0°C for 2 h; the ppt. was filtered off, washed with methanol and pentane, and dried under N2;;
DOI:10.1039/DT9920002263

Reference yield:

: 75365-55-8,97590-53-9,178457-45-9
MoCl₃(triphos)

: 75420-24-5
Mo(N₂)2((C₆H₅)2PCH₂CH₂P(C₆H₅)CH₂CH₂P(C₆H₅)2)(P(C₆H₅)3)*0.5OC₄H₈

Guidance literature:: With nitrogen; triphenylphosphine; In tetrahydrofuran; to soln. MoCl3(triphos), PPh3 in THF under N2 sodium amalgam added, mixt. stirred for 2 h; soln. filtered, THF removed, residue dissolved in benzene, soln. filtered, methanol added, solid filtered, washed with methanol, dried in vacuoand recrystd. twice by dissolving in THF, followed by methanol; elem. anal.;
DOI:10.1021/ic50215a061

Reference yield:

: 31355-55-2,39210-30-5
trichlorotris(tetrahydrofuran)molybdenum(III)

: 23582-02-7
bis(2-diphenylphosphinoethyl)phenylphosphine

: 74707-26-9,75420-24-5
Mo(N₂)2(triphos)(PPh₃)

Guidance literature:: With triphenylphosphine; In not given; Electrolysis; soln. of Mo-complex, triphos and PPh3 (molar ratio 1:1:1) in 0.5 N NBu4BF4-THF were stirred for 1 h, electrolyzed at 0°C with N2 passingover cathode;