1⁴-<4-phenyldiazenyl>-2,5,8,11-tetraoxa-1(1,2)-benzenacycloundecaphane

Base Information

Chemical Name:1⁴-<4-phenyldiazenyl>-2,5,8,11-tetraoxa-1(1,2)-benzenacycloundecaphane
CAS No.:172693-84-4
Molecular Formula:C₃₄H₅₃N₂O₈P
Molecular Weight:648.777
Hs Code.:

1<sup>4</sup>-<4-<hexadecyloxy(hydroxy)phosphoryloxy>phenyldiazenyl>-2,5,8,11-tetraoxa-1(1,2)-benzenacycloundecaphane

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1⁴-<4-phenyldiazenyl>-2,5,8,11-tetraoxa-1(1,2)-benzenacycloundecaphane

Chemical Property:

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Technology Process of 1⁴-<4-phenyldiazenyl>-2,5,8,11-tetraoxa-1(1,2)-benzenacycloundecaphane

There total 5 articles about 1⁴-<4-phenyldiazenyl>-2,5,8,11-tetraoxa-1(1,2)-benzenacycloundecaphane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 172693-85-5
1⁴-<4-phenyldiazenyl>-2,5,8,11-tetraoxa-1(1,2)-benzenacycloundecaphane

: 172693-84-4
1⁴-<4-phenyldiazenyl>-2,5,8,11-tetraoxa-1(1,2)-benzenacycloundecaphane

Guidance literature:: In methanol; water; at 25 ℃; for 0.1h; Yield given; Irradiation; other solvent: o-dichlorobenzene;

Reference yield:

: 36653-82-4,124-29-8
1-Hexadecanol

: 172693-84-4
1⁴-<4-phenyldiazenyl>-2,5,8,11-tetraoxa-1(1,2)-benzenacycloundecaphane

Guidance literature:: Multi-step reaction with 3 steps

1: phosphorus oxychloride

2: 2.) water / 1.) benzene, reflux, 60 h, 2.) 48 h

3: methanol; H₂O / 0.1 h / 25 °C / Irradiation; other solvent: o-dichlorobenzene

With water; trichlorophosphate; In methanol; water;

Reference yield:

: 78554-68-4
6,7,9,10,12,13-Hexahydro-5,8,11,14-tetraoxa-benzocyclododecen-2-ylamine

: 172693-84-4
1⁴-<4-phenyldiazenyl>-2,5,8,11-tetraoxa-1(1,2)-benzenacycloundecaphane

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) sodium nitrite, hydrochloric acid, 2.) sodium hydroxide, sodium sulfate / 2.) water, 24 h

2: 2.) water / 1.) benzene, reflux, 60 h, 2.) 48 h

3: methanol; H₂O / 0.1 h / 25 °C / Irradiation; other solvent: o-dichlorobenzene

With hydrogenchloride; sodium hydroxide; water; sodium sulfate; sodium nitrite; In methanol; water;