Benzoic acid (8R,9S,13S,14S,17S)-6-[(E)-carboxymethoxyimino]-17-hydroxy-13-methyl-7,8,9,11,12,13,14,15,16,17-decahydro-6H-cyclopenta[a]phenanthren-3-yl ester

Base Information

• Chemical Name: Benzoic acid (8R,9S,13S,14S,17S)-6-[(E)-carboxymethoxyimino]-17-hydroxy-13-methyl-7,8,9,11,12,13,14,15,16,17-decahydro-6H-cyclopenta[a]phenanthren-3-yl ester
• CAS No.: 65132-67-4
• Molecular Formula: C₂₇H₂₉NO₆
• Molecular Weight: 463.53

Synonyms:

Chemical Property of Benzoic acid (8R,9S,13S,14S,17S)-6-[(E)-carboxymethoxyimino]-17-hydroxy-13-methyl-7,8,9,11,12,13,14,15,16,17-decahydro-6H-cyclopenta[a]phenanthren-3-yl ester

Chemical Property:

Purity/Quality:

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MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Benzoic acid (8R,9S,13S,14S,17S)-6-[(E)-carboxymethoxyimino]-17-hydroxy-13-methyl-7,8,9,11,12,13,14,15,16,17-decahydro-6H-cyclopenta[a]phenanthren-3-yl ester

There total 1 articles about Benzoic acid (8R,9S,13S,14S,17S)-6-[(E)-carboxymethoxyimino]-17-hydroxy-13-methyl-7,8,9,11,12,13,14,15,16,17-decahydro-6H-cyclopenta[a]phenanthren-3-yl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(aminooxy)acetic acid hemihydrochloride (2921-14-4,7776-18-3,20295-82-3) + Benzoic acid (8R,9S,13S,14S,17S)-17-hydroxy-13-methyl-6-oxo-7,8,9,11,12,13,14,15,16,17-decahydro-6H-cyclopenta[a]phenanthren-3-yl ester → Benzoic acid (8R,9S,13S,14S,17S)-6-[(E)-carboxymethoxyimino]-17-hydroxy-13-methyl-7,8,9,11,12,13,14,15,16,17-decahydro-6H-cyclopenta[a]phenanthren-3-yl ester (65132-67-4)

Guidance literature:

With sodium acetate;

DOI:10.1016/0039-128X(77)90139-8

Reference yield:

Benzoic acid (8R,9S,13S,14S,17S)-6-[(E)-carboxymethoxyimino]-17-hydroxy-13-methyl-7,8,9,11,12,13,14,15,16,17-decahydro-6H-cyclopenta[a]phenanthren-3-yl ester (65132-67-4) → 6-keto-1,3,5(10)estratriene-3,17β-diol 6-carboxymethyloxime (35048-47-6)

Guidance literature:

With potassium hydroxide;

DOI:10.1016/0039-128X(77)90139-8

Reference yield:

Benzoic acid (8R,9S,13S,14S,17S)-6-[(E)-carboxymethoxyimino]-17-hydroxy-13-methyl-7,8,9,11,12,13,14,15,16,17-decahydro-6H-cyclopenta[a]phenanthren-3-yl ester (65132-67-4) → Benzoic acid (8R,9S,13S,14S)-6-[(E)-carboxymethoxyimino]-13-methyl-17-oxo-7,8,9,11,12,13,14,15,16,17-decahydro-6H-cyclopenta[a]phenanthren-3-yl ester

Guidance literature:

With chromium(VI) oxide; sulfuric acid;

DOI:10.1016/0039-128X(77)90139-8

upstream raw materials:

(aminooxy)acetic acid hemihydrochloride

Downstream raw materials:

6-keto-1,3,5(10)estratriene-3,17β-diol 6-carboxymethyloxime

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