4-methylphenyl-3-(trimethylstannyl)propylsulfide

Base Information

Chemical Name:4-methylphenyl-3-(trimethylstannyl)propylsulfide
CAS No.:412944-05-9
Molecular Formula:C₁₃H₂₂SSn
Molecular Weight:329.094
Hs Code.:

Synonyms:

Suppliers and Price of 4-methylphenyl-3-(trimethylstannyl)propylsulfide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 4-methylphenyl-3-(trimethylstannyl)propylsulfide

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 4-methylphenyl-3-(trimethylstannyl)propylsulfide

There total 1 articles about 4-methylphenyl-3-(trimethylstannyl)propylsulfide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.0%

: 762-73-2
trimethyl(allyl)stannane

: 106-45-6
para-thiocresol

: 412944-05-9
4-methylphenyl-3-(trimethylstannyl)propylsulfide

Guidance literature:: With dibenzoyl peroxide; In hexane; byproducts: 4-methylphenyl disulfide; Irradiation (UV/VIS); a mixt. of Sn-compound, 4-toluenethiol, benzoyl peroxide in hexane was UV-irradiated for 15 h with stirring at -50-70°C (inert atm.); the solvent was removed at reduced pressure and room temp., evacuated at100°C for some h, the residue was distilled in vac.; elem. anal.;
DOI:10.1023/A:1013197403154

Reference yield: 93.0%

: 412944-05-9
4-methylphenyl-3-(trimethylstannyl)propylsulfide

: 30066-82-1
N-chloro-p-chlorobenzenesulfonamide sodium salt

: 412944-08-2
S-(4-methylphenyl)-S-[3-(trimethylstannyl)propyl]-N-(4-chlorophenylsulfonyl)sulfonimide

Guidance literature:: In methanol; byproducts: NaCl; a soln. of Chloramine-XB in methanol was added with stirring to a soln. of sulfide in methanol, the mixt. was heated under reflux for 8 h; NaCl was filtered off, the filtrate was evapd. to dryness, treated with CH2Cl2, filtered, evapd., extd. with ether; elem. anal.;
DOI:10.1023/A:1013197403154

Reference yield: 79.0%

: 412944-05-9
4-methylphenyl-3-(trimethylstannyl)propylsulfide

: 412944-04-8
4-methylphenyl 3-(trimethylstannyl)propylsulfone

Guidance literature:: With dihydrogen peroxide; In methanol; to a soln. in methanol at 0°C dropwise was added 31% H2O2, the mixt. was stirred for 3 h at 0°C then for 6 h at room temp.; evapd. in vac. at room temp., the residue was treated with warm hexane, filtered, reduced in vol., cooled to -10°C; elem. anal.;
DOI:10.1023/A:1013197403154