C₁₁H₁₂BrNO₄

Base Information

Chemical Name:C₁₁H₁₂BrNO₄
CAS No.:1357622-45-7
Molecular Formula:C₁₁H₁₂BrNO₄
Molecular Weight:302.125
Hs Code.:

C<sub>11</sub>H<sub>12</sub>BrNO<sub>4</sub>

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₁₁H₁₂BrNO₄

Chemical Property:

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Technology Process of C₁₁H₁₂BrNO₄

There total 9 articles about C₁₁H₁₂BrNO₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1357622-43-5
(R)-2-((3-bromophenoxy)methyl)-3-formylamino-1-propanol

: 1357622-45-7
C₁₁H₁₂BrNO₄

Guidance literature:: (R)-2-((3-bromophenoxy)methyl)-3-formylamino-1-propanol; With Jones reagent; In acetone; at 0 ℃; for 2h; Inert atmosphere;

With hydrogenchloride; ammonium dihydrogen phosphate; sodium chloride; In water; acetone; pH=2; Inert atmosphere;
DOI:10.1039/c1ob06632c

Reference yield:

: 1357622-26-4
(R,E)-2-(3-bromophenoxy)methyl-5-methylhex-3-enyl acetate

: 1357622-45-7
C₁₁H₁₂BrNO₄

Guidance literature:: Multi-step reaction with 8 steps

1.1: potassium hydroxide / methanol / 0 °C

2.1: triethylamine / dichloromethane / -30 °C / Inert atmosphere

3.1: sodium azide / N,N-dimethyl-formamide / 50 °C / Inert atmosphere

4.1: triphenylphosphine / tetrahydrofuran; water / 0 - 50 °C / Inert atmosphere

5.1: dicyclohexyl-carbodiimide / dichloromethane / 0 - 20 °C / Inert atmosphere

6.1: ozone / methanol; dichloromethane / -78 °C / Inert atmosphere

6.2: -78 °C / Inert atmosphere

7.1: sodium tetrahydroborate / methanol; dichloromethane / -78 - -3 °C / Inert atmosphere

8.1: Jones reagent / acetone / 2 h / 0 °C / Inert atmosphere

8.2: pH 2 / Inert atmosphere

With sodium tetrahydroborate; Jones reagent; sodium azide; ozone; triethylamine; dicyclohexyl-carbodiimide; triphenylphosphine; potassium hydroxide; In tetrahydrofuran; methanol; dichloromethane; water; N,N-dimethyl-formamide; acetone;
DOI:10.1039/c1ob06632c

Reference yield:

: 1357622-40-2
(S,E)-2-((3-bromophenoxy)methyl)-5-methylhex-3-en-1-ol

: 1357622-45-7
C₁₁H₁₂BrNO₄

Guidance literature:: Multi-step reaction with 7 steps

1.1: triethylamine / dichloromethane / -30 °C / Inert atmosphere

2.1: sodium azide / N,N-dimethyl-formamide / 50 °C / Inert atmosphere

3.1: triphenylphosphine / tetrahydrofuran; water / 0 - 50 °C / Inert atmosphere

4.1: dicyclohexyl-carbodiimide / dichloromethane / 0 - 20 °C / Inert atmosphere

5.1: ozone / methanol; dichloromethane / -78 °C / Inert atmosphere

5.2: -78 °C / Inert atmosphere

6.1: sodium tetrahydroborate / methanol; dichloromethane / -78 - -3 °C / Inert atmosphere

7.1: Jones reagent / acetone / 2 h / 0 °C / Inert atmosphere

7.2: pH 2 / Inert atmosphere

With sodium tetrahydroborate; Jones reagent; sodium azide; ozone; triethylamine; dicyclohexyl-carbodiimide; triphenylphosphine; In tetrahydrofuran; methanol; dichloromethane; water; N,N-dimethyl-formamide; acetone;
DOI:10.1039/c1ob06632c