5b,7b-diaza-3b,9b-dibora-4,9-diphenylbenzo[ghi]perylene

Base Information

• Chemical Name: 5b,7b-diaza-3b,9b-dibora-4,9-diphenylbenzo[ghi]perylene
• CAS No.: 1227401-20-8
• Molecular Formula: C₃₂H₂₄B₂N₂
• Molecular Weight: 458.178
• Mol file: 1227401-20-8.mol

Synonyms:

Chemical Property of 5b,7b-diaza-3b,9b-dibora-4,9-diphenylbenzo[ghi]perylene

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 5b,7b-diaza-3b,9b-dibora-4,9-diphenylbenzo[ghi]perylene

There total 1 articles about 5b,7b-diaza-3b,9b-dibora-4,9-diphenylbenzo[ghi]perylene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 3.0%

(C5H3B(Cl)(CH3)(Si(CH3)3))2 (1227279-45-9) + 3,6-bis(phenylethynyl)pyridazine (77778-16-6) → 5b,7b-diaza-3b,9b-dibora-4,9-diphenylbenzo[ghi]perylene (1227401-20-8)

Guidance literature:

platinum(II) chloride; In toluene; mixt. of soln. was stirred at 45°C for 48 h, volatiles were removed in vac. and crude residue was re-dissolved and transferred onto PtCl2, mixt. was stirred at 100°C for 24 h; volatiles were removed, flash chromy. (Al2O3);

DOI:10.1139/V10-009

upstream raw materials:

(C₅H₃B(Cl)(CH₃)(Si(CH₃)3))2

3,6-bis(phenylethynyl)pyridazine