C₈H₁₁N*C₁₇H₁₅ClO₃

Base Information

Chemical Name:C₈H₁₁N*C₁₇H₁₅ClO₃
CAS No.:1268246-53-2
Molecular Formula:C₈H₁₁N*C₁₇H₁₅ClO₃
Molecular Weight:423.939
Hs Code.:

C<sub>8</sub>H<sub>11</sub>N*C<sub>17</sub>H<sub>15</sub>ClO<sub>3</sub>

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₈H₁₁N*C₁₇H₁₅ClO₃

Chemical Property:

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Technology Process of C₈H₁₁N*C₁₇H₁₅ClO₃

There total 22 articles about C₈H₁₁N*C₁₇H₁₅ClO₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1268246-52-1
C₁₇H₁₅ClO₃

: 2627-86-3
(S)-1-phenyl-ethylamine

: 1268246-53-2
C₈H₁₁N*C₁₇H₁₅ClO₃

Guidance literature:: In toluene; Reflux;

Reference yield:

: 96534-02-0
3-(diethyoxyphosphorylmethyl)benzoic acid methyl ester

: 1268246-53-2
C₈H₁₁N*C₁₇H₁₅ClO₃

Guidance literature:: Multi-step reaction with 11 steps

1.1: sodium hydride / tetrahydrofuran; mineral oil / 0.5 h / 0 °C

1.2: 0 - 20 °C

2.1: triethylamine / dmap / dichloromethane / 1 h / 20 °C

3.1: diethylzinc / dichloromethane; hexane / 0.5 h / -78 °C

3.2: 0.5 h / -30 °C

3.3: 20 °C

4.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 0.17 h / 20 °C

5.1: potassium carbonate / N,N-dimethyl-formamide / 60 °C

6.1: water; lithium hydroxide monohydrate / tetrahydrofuran / 24 h / 20 °C

7.1: CHIRALPAK AD-H / hexane; ethanol; acetic acid / Resolution of racemate

8.1: hydrogenchloride / 1,4-dioxane / 4 h / 85 °C

9.1: palladium diacetate / diethyl ether / -50 - 20 °C / Inert atmosphere

10.1: water; lithium hydroxide monohydrate / tetrahydrofuran / 4 h / 40 °C

10.2: pH 4

11.1: toluene / Reflux

With hydrogenchloride; lithium hydroxide monohydrate; tetrabutyl ammonium fluoride; water; diethylzinc; sodium hydride; potassium carbonate; triethylamine; dmap; palladium diacetate; In tetrahydrofuran; 1,4-dioxane; diethyl ether; ethanol; hexane; dichloromethane; acetic acid; N,N-dimethyl-formamide; toluene; mineral oil;

Reference yield:

: 1459-93-4
dimethyl Isophthalate

: 1268246-53-2
C₈H₁₁N*C₁₇H₁₅ClO₃

Guidance literature:: Multi-step reaction with 15 steps

1.1: sodium hydroxide / methanol / 20 °C

2.1: borane-THF / tetrahydrofuran / 0 - 20 °C / Inert atmosphere

3.1: phosphorus tribromide / diethyl ether / 2 h

4.1: 4 h / 175 °C

5.1: sodium hydride / tetrahydrofuran; mineral oil / 0.5 h / 0 °C

5.2: 0 - 20 °C

6.1: triethylamine / dmap / dichloromethane / 1 h / 20 °C

7.1: diethylzinc / dichloromethane; hexane / 0.5 h / -78 °C

7.2: 0.5 h / -30 °C

7.3: 20 °C

8.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 0.17 h / 20 °C

9.1: potassium carbonate / N,N-dimethyl-formamide / 60 °C

10.1: water; lithium hydroxide monohydrate / tetrahydrofuran / 24 h / 20 °C

11.1: CHIRALPAK AD-H / hexane; ethanol; acetic acid / Resolution of racemate

12.1: hydrogenchloride / 1,4-dioxane / 4 h / 85 °C

13.1: palladium diacetate / diethyl ether / -50 - 20 °C / Inert atmosphere

14.1: water; lithium hydroxide monohydrate / tetrahydrofuran / 4 h / 40 °C

14.2: pH 4

15.1: toluene / Reflux

With hydrogenchloride; borane-THF; lithium hydroxide monohydrate; tetrabutyl ammonium fluoride; water; diethylzinc; phosphorus tribromide; sodium hydride; potassium carbonate; triethylamine; sodium hydroxide; dmap; palladium diacetate; In tetrahydrofuran; 1,4-dioxane; methanol; diethyl ether; ethanol; hexane; dichloromethane; acetic acid; N,N-dimethyl-formamide; toluene; mineral oil;