1-benzoyloxy-2-benzoyloxymethyl-3-fluoro-4-triphenylmethoxybutane

Base Information

Chemical Name:1-benzoyloxy-2-benzoyloxymethyl-3-fluoro-4-triphenylmethoxybutane
CAS No.:119117-71-4
Molecular Formula:C₃₈H₃₃FO₅
Molecular Weight:588.675
Hs Code.:

Synonyms:

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Chemical Property of 1-benzoyloxy-2-benzoyloxymethyl-3-fluoro-4-triphenylmethoxybutane

Chemical Property:

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Technology Process of 1-benzoyloxy-2-benzoyloxymethyl-3-fluoro-4-triphenylmethoxybutane

There total 7 articles about 1-benzoyloxy-2-benzoyloxymethyl-3-fluoro-4-triphenylmethoxybutane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 61.0%

: 119117-70-3
4-benzoyloxy-3-benzoyloxymethyl-1-triphenylmethoxybutan-2-ol

: 119117-71-4
1-benzoyloxy-2-benzoyloxymethyl-3-fluoro-4-triphenylmethoxybutane

Guidance literature:: With diethylamino-sulfur trifluoride; triethylamine; In tetrahydrofuran; N,N-dimethyl-formamide; for 20h; Ambient temperature;

Reference yield:

: 98-88-4
benzoyl chloride

: 119117-71-4
1-benzoyloxy-2-benzoyloxymethyl-3-fluoro-4-triphenylmethoxybutane

Guidance literature:: Multi-step reaction with 4 steps

1: 67 percent / 4-N,N-dimethylaminopyridine / pyridine / 42 h / Ambient temperature

2: 90 percent / 5M hydrochloric acid, H₂ / 5percent palladium charcoal / tetrahydrofuran; H₂O / 7 h / Ambient temperature

3: 85 percent / pyridine / 4 h / 70 °C

4: 61 percent / triethylamine, diethylaminosulphur trifluoride / tetrahydrofuran; dimethylformamide / 20 h / Ambient temperature

With pyridine; hydrogenchloride; dmap; diethylamino-sulfur trifluoride; hydrogen; triethylamine; palladium on activated charcoal; In tetrahydrofuran; pyridine; water; N,N-dimethyl-formamide;

Reference yield:

: 119117-67-8
3,4-dibenzyloxy-2-hydroxymethylbutan-1-ol

: 119117-71-4
1-benzoyloxy-2-benzoyloxymethyl-3-fluoro-4-triphenylmethoxybutane

Guidance literature:: Multi-step reaction with 4 steps

1: 67 percent / 4-N,N-dimethylaminopyridine / pyridine / 42 h / Ambient temperature

2: 90 percent / 5M hydrochloric acid, H₂ / 5percent palladium charcoal / tetrahydrofuran; H₂O / 7 h / Ambient temperature

3: 85 percent / pyridine / 4 h / 70 °C

4: 61 percent / triethylamine, diethylaminosulphur trifluoride / tetrahydrofuran; dimethylformamide / 20 h / Ambient temperature

With pyridine; hydrogenchloride; dmap; diethylamino-sulfur trifluoride; hydrogen; triethylamine; palladium on activated charcoal; In tetrahydrofuran; pyridine; water; N,N-dimethyl-formamide;