C₉H₁₀ClNO₃

Base Information

Chemical Name:C₉H₁₀ClNO₃
CAS No.:1432589-63-3
Molecular Formula:C₉H₁₀ClNO₃
Molecular Weight:215.636
Hs Code.:

C<sub>9</sub>H<sub>10</sub>ClNO<sub>3</sub>

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₉H₁₀ClNO₃

Chemical Property:

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Technology Process of C₉H₁₀ClNO₃

There total 3 articles about C₉H₁₀ClNO₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 50-00-0,30525-89-4,61233-19-0
formaldehyd

: 140378-05-8
2-(3-chlorophenyl)-1-nitroethane

: 1432589-63-3
C₉H₁₀ClNO₃

Guidance literature:: formaldehyd; 2-(3-chlorophenyl)-1-nitroethane; With potassium hydroxide; In methanol; at 25 ℃; for 1.5h; pH=8 - 9;

With sulfuric acid; In methanol; at 25 ℃; for 1.5h; pH=4;
DOI:10.1002/adsc.201400851

Reference yield:

: 5182-44-5
2-(3-chlorophenyl)ethanol

: 1432589-63-3
C₉H₁₀ClNO₃

Guidance literature:: Multi-step reaction with 3 steps

1.1: carbon tetrabromide; triphenylphosphine / dichloromethane / 0 - 25 °C

2.1: sodium nitrite / dimethyl sulfoxide / 2 h / 20 °C

3.1: potassium hydroxide / methanol / 1.5 h / 25 °C / pH 8 - 9

3.2: 1.5 h / 25 °C / pH 4

With carbon tetrabromide; triphenylphosphine; potassium hydroxide; sodium nitrite; In methanol; dichloromethane; dimethyl sulfoxide;
DOI:10.1002/adsc.201400851

Reference yield:

: 16799-05-6
2-(3-chlorophenyl)ethyl bromide

: 1432589-63-3
C₉H₁₀ClNO₃

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium nitrite / dimethyl sulfoxide / 2 h / 20 °C

2.1: potassium hydroxide / methanol / 1.5 h / 25 °C / pH 8 - 9

2.2: 1.5 h / 25 °C / pH 4

With potassium hydroxide; sodium nitrite; In methanol; dimethyl sulfoxide;
DOI:10.1002/adsc.201400851