D-Glucit-1.2;3.4;5.6-tricarbonat

Base Information

• Chemical Name: D-Glucit-1.2;3.4;5.6-tricarbonat
• CAS No.: 31685-57-1
• Molecular Formula: C₉H₈O₉
• Molecular Weight: 260.157
• Mol file: 31685-57-1.mol

Synonyms:

Chemical Property of D-Glucit-1.2;3.4;5.6-tricarbonat

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of D-Glucit-1.2;3.4;5.6-tricarbonat

There total 1 articles about D-Glucit-1.2;3.4;5.6-tricarbonat which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

D-sorbitol (50-70-4) + carbon dioxide (124-38-9,18923-20-1) + 2-methyl-but-3-yn-2-ol (115-19-5) → D-Glucit-1.2;3.4;5.6-tricarbonat (31685-55-9,31685-56-0,31685-57-1,34022-00-9) + 3-Hydroxy-3-methyl-2-butanone (115-22-0)

Guidance literature:

carbon dioxide; 2-methyl-but-3-yn-2-ol; With C₁₅H₁₈N₂O₂; In acetonitrile; at 25 ℃; for 24h; under 760.051 Torr; Inert atmosphere; Schlenk technique;

D-sorbitol; With 1-methyl-2,3,4,6,7,8-hexahydro-1H-pyrimido[1,2-a]pyrimidine; In N,N-dimethyl-formamide; at 25 ℃; for 24h; stereoselective reaction; Inert atmosphere; Schlenk technique;

DOI:10.1039/c9gc03013a

upstream raw materials:

D-sorbitol

carbon dioxide

2-methyl-but-3-yn-2-ol