Technology Process of C60H66FN6O18P
There total 10 articles about C60H66FN6O18P which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
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Multi-step reaction with 3 steps
1: 75 percent / pyridine / CH2Cl2 / 1 h
2: 70 percent / diisopropylammonium tetrazolide / CH2Cl2 / 16 h
3: tetrazole / acetonitrile / 0.83 h
With
pyridine; 1H-tetrazole; N,N-diisopropylamine tetrazolide;
In
dichloromethane; acetonitrile;
DOI:10.1021/jo9614607
- Guidance literature:
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Multi-step reaction with 5 steps
1: 73 percent / camphor-10-sulfonic acid / CH2Cl2 / 20 h
2: 76 percent / Et3N*HF / tetrahydrofuran
3: 75 percent / pyridine / CH2Cl2 / 1 h
4: 70 percent / diisopropylammonium tetrazolide / CH2Cl2 / 16 h
5: tetrazole / acetonitrile / 0.83 h
With
pyridine; 1H-tetrazole; camphor-10-sulfonic acid; N,N-diisopropylamine tetrazolide; triethylamine hydrofluoride;
In
tetrahydrofuran; dichloromethane; acetonitrile;
DOI:10.1021/jo9614607
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1-((2R,3R,3aS,9aR)-3-Allyl-5,5,7,7-tetraisopropyl-tetrahydro-1,4,6,8-tetraoxa-5,7-disila-cyclopentacycloocten-2-yl)-4-hydroxy-1H-pyrimidin-2-one
- Guidance literature:
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Multi-step reaction with 8 steps
1: 99.6 percent / N-methylmorpholine N-oxide, OsO4 / acetone; H2O / 1.5 h
2: NaIO4 / dioxane; H2O / 0.17 h
3: 100 percent / NaBH4 / methanol / 0.33 h / 0 °C
4: 73 percent / camphor-10-sulfonic acid / CH2Cl2 / 20 h
5: 76 percent / Et3N*HF / tetrahydrofuran
6: 75 percent / pyridine / CH2Cl2 / 1 h
7: 70 percent / diisopropylammonium tetrazolide / CH2Cl2 / 16 h
8: tetrazole / acetonitrile / 0.83 h
With
pyridine; 1H-tetrazole; sodium tetrahydroborate; sodium periodate; osmium(VIII) oxide; camphor-10-sulfonic acid; N,N-diisopropylamine tetrazolide; 4-methylmorpholine N-oxide; triethylamine hydrofluoride;
In
tetrahydrofuran; 1,4-dioxane; methanol; dichloromethane; water; acetone; acetonitrile;
DOI:10.1021/jo9614607