Technology Process of C35H47NO5
There total 4 articles about C35H47NO5 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: 78 percent / TsOH; CH(OMe)3 / methanol
2.1: 87 percent / (COCl)2; Me2SO / CH2Cl2
3.1: 70 percent / aq. NaClO2; NaHPO4; 2-methyl-2-butene / 2-methyl-propan-2-ol
4.1: 2,4,6-triisopropylbenzenesulfonyl chloride; Et3N; DMAP / CH2Cl2
4.2: CH2Cl2
With
dmap; sodium chlorite; 2,4,6-triisopropylphenylsulfonyl chloride; 2-methyl-but-2-ene; oxalyl dichloride; camphor-10-sulfonic acid; toluene-4-sulfonic acid; dimethyl sulfoxide; triethylamine; trimethyl orthoformate;
In
methanol; dichloromethane; tert-butyl alcohol;
2.1: Swern oxidation;
DOI:10.1016/S0960-894X(02)00020-3
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: 70 percent / aq. NaClO2; NaHPO4; 2-methyl-2-butene / 2-methyl-propan-2-ol
2.1: 2,4,6-triisopropylbenzenesulfonyl chloride; Et3N; DMAP / CH2Cl2
2.2: CH2Cl2
With
dmap; sodium chlorite; 2,4,6-triisopropylphenylsulfonyl chloride; 2-methyl-but-2-ene; camphor-10-sulfonic acid; triethylamine;
In
dichloromethane; tert-butyl alcohol;
DOI:10.1016/S0960-894X(02)00020-3
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: 87 percent / (COCl)2; Me2SO / CH2Cl2
2.1: 70 percent / aq. NaClO2; NaHPO4; 2-methyl-2-butene / 2-methyl-propan-2-ol
3.1: 2,4,6-triisopropylbenzenesulfonyl chloride; Et3N; DMAP / CH2Cl2
3.2: CH2Cl2
With
dmap; sodium chlorite; 2,4,6-triisopropylphenylsulfonyl chloride; 2-methyl-but-2-ene; oxalyl dichloride; camphor-10-sulfonic acid; dimethyl sulfoxide; triethylamine;
In
dichloromethane; tert-butyl alcohol;
1.1: Swern oxidation;
DOI:10.1016/S0960-894X(02)00020-3