5-Iodo-4-methyl-2-nitroaniline

Base Information

Chemical Name:5-Iodo-4-methyl-2-nitroaniline
CAS No.:97113-38-7
Molecular Formula:C₇H₇IN₂O₂
Molecular Weight:278.049
Hs Code.:
DSSTox Substance ID:DTXSID201296939
Mol file:97113-38-7.mol

Synonyms:5-iodo-4-methyl-2-nitroaniline;97113-38-7;MFCD25969656;DTXSID201296939;5-Iodo-4-methyl-2-nitrobenzenamine;AC7470;SB81992;Benzenamine, 5-iodo-4-methyl-2-nitro-;SY238258;A917325

Suppliers and Price of 5-Iodo-4-methyl-2-nitroaniline

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Chemcia Scientific
5-Iodo-4-methyl-2-nitro-phenylamine ＞95%
2.5 G
$ 795.00

Chemcia Scientific
5-Iodo-4-methyl-2-nitro-phenylamine ＞95%
0.5 G
$ 275.00

AK Scientific
5-Iodo-4-methyl-2-nitroaniline
10g
$ 1268.00

AK Scientific
5-Iodo-4-methyl-2-nitroaniline
1g
$ 323.00

Total 6 raw suppliers

Chemical Property of 5-Iodo-4-methyl-2-nitroaniline

Chemical Property:

XLogP3:2.6
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:0
Exact Mass:277.95523
Heavy Atom Count:12
Complexity:183

Purity/Quality:

97% ^*data from raw suppliers

5-Iodo-4-methyl-2-nitro-phenylamine ＞95% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CC1=CC(=C(C=C1I)N)[N+](=O)[O-]

Technology Process of 5-Iodo-4-methyl-2-nitroaniline

There total 2 articles about 5-Iodo-4-methyl-2-nitroaniline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 97113-37-6
5-iodo-4-methyl-2-nitroacetanilide

: 97113-38-7
5-iodo-4-methyl-2-nitroaniline

Guidance literature:: With hydrogenchloride; In ethanol; for 1.5h; Yield given; Heating;
DOI:10.1021/jm00148a003

Reference yield:

: 97113-36-5
3-iodo-4-methylacetanilide

: 97113-38-7
5-iodo-4-methyl-2-nitroaniline

Guidance literature:: Multi-step reaction with 2 steps

1: fuming HNO₃ / acetic anhydride / 1 h / Ambient temperature

2: conc. aq. HCl / ethanol / 1.5 h / Heating

With hydrogenchloride; nitric acid; In ethanol; acetic anhydride;
DOI:10.1021/jm00148a003

Reference yield:

: 97113-38-7
5-iodo-4-methyl-2-nitroaniline

: 97112-84-0
2-Amino-4-methyl-5-piperidin-1-yl-benzonitrile

Guidance literature:: Multi-step reaction with 3 steps

1: aq. HCl, NaNO₂ / 1.) acetone, 2.) acetone, water

2: 73 percent / dimethylformamide / 0.5 h / 50 °C

3: 91 percent / conc. aq. HCl, SnCl₂*2H₂O / 2 h / Ambient temperature

With hydrogenchloride; tin(ll) chloride; sodium nitrite; In N,N-dimethyl-formamide;
DOI:10.1021/jm00148a003