3-dichloro-5,5-difluoro-7-methoxy-10-(4-(2-methoxy-2-oxoethoxy)-2,6-dimethylphenyl)-5H-dipyrrolo[1,2-c:2',1'-f][1,3,2]diazaborinin-4-ium-5-uide

Base Information

Chemical Name:3-dichloro-5,5-difluoro-7-methoxy-10-(4-(2-methoxy-2-oxoethoxy)-2,6-dimethylphenyl)-5H-dipyrrolo[1,2-c:2',1'-f][1,3,2]diazaborinin-4-ium-5-uide
CAS No.:1309582-36-2
Molecular Formula:C₂₁H₂₀BClF₂N₂O₄
Molecular Weight:448.662
Hs Code.:

3-dichloro-5,5-difluoro-7-methoxy-10-(4-(2-methoxy-2-oxoethoxy)-2,6-dimethylphenyl)-5H-dipyrrolo[1,2-c:2',1'-f][1,3,2]diazaborinin-4-ium-5-uide

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Chemical Property of 3-dichloro-5,5-difluoro-7-methoxy-10-(4-(2-methoxy-2-oxoethoxy)-2,6-dimethylphenyl)-5H-dipyrrolo[1,2-c:2',1'-f][1,3,2]diazaborinin-4-ium-5-uide

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Technology Process of 3-dichloro-5,5-difluoro-7-methoxy-10-(4-(2-methoxy-2-oxoethoxy)-2,6-dimethylphenyl)-5H-dipyrrolo[1,2-c:2',1'-f][1,3,2]diazaborinin-4-ium-5-uide

There total 1 articles about 3-dichloro-5,5-difluoro-7-methoxy-10-(4-(2-methoxy-2-oxoethoxy)-2,6-dimethylphenyl)-5H-dipyrrolo[1,2-c:2',1'-f][1,3,2]diazaborinin-4-ium-5-uide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 1309582-44-2
3,7-dichloro-5,5-difluoro-10-(4-(2-methoxy-2-oxoethoxy)-2,6-dimethylphenyl)-5H-dipyrrolo[1,2-c:2',1'-f][1,3,2]diazaborinin-4-ium-5-uide

: 124-41-4
sodium methylate

: 1309582-36-2
3-dichloro-5,5-difluoro-7-methoxy-10-(4-(2-methoxy-2-oxoethoxy)-2,6-dimethylphenyl)-5H-dipyrrolo[1,2-c:2',1'-f][1,3,2]diazaborinin-4-ium-5-uide

Guidance literature:: In tetrahydrofuran; methanol; (N2); addn. of methanolic soln. of sodium methoxide to soln. of boron compd. in THF at 0°C over 2.5 h, keeping at 0°C for 4 h; evapn., addn. of water and CH2Cl2, separating CH2Cl2 layer, drying over Na2SO4, filtration, drying in vac., chromy. (silica, CH2Cl2), NMR and MS;
DOI:10.1021/ja2004158

Reference yield:

: 1309582-36-2
3-dichloro-5,5-difluoro-7-methoxy-10-(4-(2-methoxy-2-oxoethoxy)-2,6-dimethylphenyl)-5H-dipyrrolo[1,2-c:2',1'-f][1,3,2]diazaborinin-4-ium-5-uide

: 1309582-38-4
3-(bis(2-((2-(ethylthio)ethyl)thio)ethyl)amino)-10-(4-(2-carboxmethoxy)-2,6-dimethylphenyl)-5,5-difluoro-7-methoxy-5H-dipyrrolo[1,2-c:2',1'-f][1,3,2]diazaborinin-4-ium-5-uide

Guidance literature:: Multi-step reaction with 2 steps

1: acetonitrile

2: LiOH / methanol; tetrahydrofuran

With LiOH; In tetrahydrofuran; methanol; acetonitrile;
DOI:10.1021/ja2004158

Reference yield:

: 1309582-36-2
3-dichloro-5,5-difluoro-7-methoxy-10-(4-(2-methoxy-2-oxoethoxy)-2,6-dimethylphenyl)-5H-dipyrrolo[1,2-c:2',1'-f][1,3,2]diazaborinin-4-ium-5-uide

: 1309582-39-5
((C₆H₅)3PCH₂CH₂NHCOCH₂OC₆H₂(CH₃)2C(C₄H₂N(N(CH₂CH₂SCH₂CH₂SCH₂CH₃)2))(C₄H₂NOCH₃))BF₂⁽¹⁺⁾

Guidance literature:: Multi-step reaction with 3 steps

1: acetonitrile

2: LiOH / methanol; tetrahydrofuran

3: CH₃CH₂N(CH(CH₃)2)2; [C₅H₃N₄OC(N(CH₃)2)2]PF₆ / dichloromethane

With LiOH; CH₃CH₂N(CH(CH₃)2)2; [C₅H₃N₄OC(N(CH₃)2)2]PF₆; In tetrahydrofuran; methanol; dichloromethane; acetonitrile;
DOI:10.1021/ja2004158