N-phenyl-N-(piperidin-2-ylmethyl)indan-2-yl-amine

Base Information

Chemical Name:N-phenyl-N-(piperidin-2-ylmethyl)indan-2-yl-amine
CAS No.:313257-62-4
Molecular Formula:C₂₁H₂₆N₂
Molecular Weight:306.451
Hs Code.:

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Chemical Property of N-phenyl-N-(piperidin-2-ylmethyl)indan-2-yl-amine

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Technology Process of N-phenyl-N-(piperidin-2-ylmethyl)indan-2-yl-amine

There total 6 articles about N-phenyl-N-(piperidin-2-ylmethyl)indan-2-yl-amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 3433-37-2
piperidin-2-ylmethanol

: 313257-62-4
N-phenyl-N-(piperidin-2-ylmethyl)indan-2-yl-amine

Guidance literature:: Multi-step reaction with 4 steps

1.1: potassium carbonate / N,N-dimethyl-formamide / 16 h / 0 - 20 °C

2.1: thionyl chloride / chloroform / 2 h / 0 °C / Reflux

3.1: sodium amide / toluene / 3 h / 0 - 20 °C

3.2: 16 h / Reflux

4.1: ammonium formate / palladium 10% on activated carbon / methanol / 3 h / Reflux; Inert atmosphere

With thionyl chloride; ammonium formate; potassium carbonate; sodium amide; palladium 10% on activated carbon; In methanol; chloroform; N,N-dimethyl-formamide; toluene;

Reference yield:

: 129437-88-3
1-benzyl-2-(chloromethyl)piperidine

: 313257-62-4
N-phenyl-N-(piperidin-2-ylmethyl)indan-2-yl-amine

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium amide / toluene / 3 h / 0 - 20 °C

1.2: 16 h / Reflux

2.1: ammonium formate / palladium 10% on activated carbon / methanol / 3 h / Reflux; Inert atmosphere

With ammonium formate; sodium amide; palladium 10% on activated carbon; In methanol; toluene;

Reference yield:

: 137650-02-3,85387-43-5
(1-benzylpiperidin-2-yl)methanol

: 313257-62-4
N-phenyl-N-(piperidin-2-ylmethyl)indan-2-yl-amine

Guidance literature:: Multi-step reaction with 3 steps

1.1: thionyl chloride / chloroform / 2 h / 0 °C / Reflux

2.1: sodium amide / toluene / 3 h / 0 - 20 °C

2.2: 16 h / Reflux

3.1: ammonium formate / palladium 10% on activated carbon / methanol / 3 h / Reflux; Inert atmosphere

With thionyl chloride; ammonium formate; sodium amide; palladium 10% on activated carbon; In methanol; chloroform; toluene;