ethyl 3-(4-methoxyphenyl)-4-methyl-5-methylthio furan-2-carboxylate

Base Information

• Chemical Name: ethyl 3-(4-methoxyphenyl)-4-methyl-5-methylthio furan-2-carboxylate
• CAS No.: 128031-85-6
• Molecular Formula: C₁₆H₁₈O₄S
• Molecular Weight: 306.383
• Mol file: 128031-85-6.mol

Synonyms:

Chemical Property of ethyl 3-(4-methoxyphenyl)-4-methyl-5-methylthio furan-2-carboxylate

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

Useful:

Technology Process of ethyl 3-(4-methoxyphenyl)-4-methyl-5-methylthio furan-2-carboxylate

There total 1 articles about ethyl 3-(4-methoxyphenyl)-4-methyl-5-methylthio furan-2-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 40.0%

1-(4-Methoxy-phenyl)-2-methyl-3,3-bis-methylsulfanyl-propenone (61541-61-5) + ethyl bromoacetate (105-36-2) → ethyl 3-(4-methoxyphenyl)-4-methyl-5-methylthio furan-2-carboxylate (128031-85-6)

Guidance literature:

With ammonium chloride; lithium hexamethyldisilazane; In tetrahydrofuran; for 12h; Ambient temperature;

DOI:10.1016/S0040-4020(01)89224-3

upstream raw materials:

1-(4-Methoxy-phenyl)-2-methyl-3,3-bis-methylsulfanyl-propenone

ethyl bromoacetate