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C52H52O18

Base Information
  • Chemical Name:C52H52O18
  • CAS No.:329327-17-5
  • Molecular Formula:C52H52O18
  • Molecular Weight:964.974
  • Hs Code.:
C<sub>52</sub>H<sub>52</sub>O<sub>18</sub>

Synonyms:

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Chemical Property of C52H52O18
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Technology Process of C52H52O18

There total 1 articles about C52H52O18 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
With triphenylphosphine hydrobromide; In dichloromethane; at 20 ℃; for 40h;
DOI:10.1039/b007267m
Guidance literature:
With sodium methylate; In tetrahydrofuran; methanol; at 20 ℃; for 0.5h;
DOI:10.1039/b007267m
Guidance literature:
Multi-step reaction with 12 steps
1: 18.27 g / NaOMe / methanol; tetrahydrofuran / 0.5 h / 20 °C
2: 62.8 percent / imidazole; Et3N / hexamethylphosphoric acid triamide / 60 h / 20 °C
3: 73 percent / pyridine / acetonitrile / 1.33 h / 20 °C
4: 41.7 percent / 1H-tetraole; DMAP; pyridine / acetonitrile / 0.75 h / 20 °C
5: ClCH2CO2H; pyrrole / CH2Cl2 / 0.25 h / 20 °C
6: imidazole / dimethylformamide / 7 h / 80 °C
7: PTSA*H2O / CH2Cl2; methanol / 2 h / 20 °C
8: MeNH2 / ethanol / 0.75 h / 20 °C
9: PTSA*H2O / 1 h / 20 °C
10: Et4NF; Et4NOH / aq. ethanol; acetonitrile / 16 h / Heating
11: NaH / dimethylformamide / 2.5 h / 20 °C
12: PTSA*H2O / CH2Cl2; aq. methanol / 2 h / 20 °C
With pyridine; 1H-imidazole; 1H-tetrazole; dmap; pyrrole; sodium methylate; tetraethylammonium hydroxide; sodium hydride; tetraethylammonium fluoride; toluene-4-sulfonic acid; triethylamine; chloroacetic acid; methylamine; In tetrahydrofuran; methanol; N,N,N,N,N,N-hexamethylphosphoric triamide; ethanol; dichloromethane; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1039/b007267m
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