C₇H₈O₃S*C₂₉H₃₇N₃O₃

Base Information

Chemical Name:C₇H₈O₃S*C₂₉H₃₇N₃O₃
CAS No.:1267498-35-0
Molecular Formula:C₇H₈O₃S*C₂₉H₃₇N₃O₃
Molecular Weight:647.836
Hs Code.:

C<sub>7</sub>H<sub>8</sub>O<sub>3</sub>S*C<sub>29</sub>H<sub>37</sub>N<sub>3</sub>O<sub>3</sub>

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Chemical Property of C₇H₈O₃S*C₂₉H₃₇N₃O₃

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Technology Process of C₇H₈O₃S*C₂₉H₃₇N₃O₃

There total 7 articles about C₇H₈O₃S*C₂₉H₃₇N₃O₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 886041-53-8
3-cyclohexyl-2-{2-[(2S)-oxiran-2-ylmethoxy]phenyl}-1H-indole-6-carboxylic acid methyl ester

: 1267498-35-0
C₇H₈O₃S*C₂₉H₃₇N₃O₃

Guidance literature:: Multi-step reaction with 6 steps

1.1: caesium carbonate / N,N-dimethyl acetamide / 2.5 h / 65 °C / Large scale reaction

2.1: pyridine; dimethyl sulfoxide; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; trifluoroacetic acid

3.1: sodium tris(acetoxy)borohydride / DCE

4.1: palladium on activated charcoal; sodium acetate / methanol

5.1: water; sodium hydroxide / methanol / 3 h / 72 °C / Large scale reaction

5.2: 20 - 25 °C / Large scale reaction

5.3: Large scale reaction

6.1: dichloromethane; acetonitrile / Large scale reaction

With pyridine; palladium on activated charcoal; water; sodium acetate; sodium tris(acetoxy)borohydride; caesium carbonate; dimethyl sulfoxide; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; trifluoroacetic acid; sodium hydroxide; In methanol; DCE; dichloromethane; N,N-dimethyl acetamide; acetonitrile; 2.1: modified Pfitzner-Moffatt conditions reaction;
DOI:10.1021/op200002u

Reference yield:

: 886041-55-0
methyl 14-cyclohexyl-7-oxo-7,8-dihydro-6H-indolo[1,2-e][1,5]benzoxazocine-11-carboxylate

: 1267498-35-0
C₇H₈O₃S*C₂₉H₃₇N₃O₃

Guidance literature:: Multi-step reaction with 4 steps

1.1: sodium tris(acetoxy)borohydride / DCE

2.1: palladium on activated charcoal; sodium acetate / methanol

3.1: water; sodium hydroxide / methanol / 3 h / 72 °C / Large scale reaction

3.2: 20 - 25 °C / Large scale reaction

3.3: Large scale reaction

4.1: dichloromethane; acetonitrile / Large scale reaction

With palladium on activated charcoal; water; sodium acetate; sodium tris(acetoxy)borohydride; sodium hydroxide; In methanol; DCE; dichloromethane; acetonitrile;
DOI:10.1021/op200002u

Reference yield:

: 886041-54-9
methyl (7S)-14-cyclohexyl-7-hydroxy-7,8-dihydro-6H-indolo[1,2-e][1,5]benzoxazocine-11-carboxylate

: 1267498-35-0
C₇H₈O₃S*C₂₉H₃₇N₃O₃

Guidance literature:: Multi-step reaction with 5 steps

1.1: pyridine; dimethyl sulfoxide; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; trifluoroacetic acid

2.1: sodium tris(acetoxy)borohydride / DCE

3.1: palladium on activated charcoal; sodium acetate / methanol

4.1: water; sodium hydroxide / methanol / 3 h / 72 °C / Large scale reaction

4.2: 20 - 25 °C / Large scale reaction

4.3: Large scale reaction

5.1: dichloromethane; acetonitrile / Large scale reaction

With pyridine; palladium on activated charcoal; water; sodium acetate; sodium tris(acetoxy)borohydride; dimethyl sulfoxide; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; trifluoroacetic acid; sodium hydroxide; In methanol; DCE; dichloromethane; acetonitrile; 1.1: modified Pfitzner-Moffatt conditions reaction;
DOI:10.1021/op200002u