Cyclopropyl-Z-phenylalanine methyl ester hydrochloride

Base Information

Chemical Name:Cyclopropyl-Z-phenylalanine methyl ester hydrochloride
CAS No.:82112-04-7
Molecular Formula:C₁₁H₁₃NO₂*ClH
Molecular Weight:227.691
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Cyclopropyl-Z-phenylalanine methyl ester hydrochloride

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Technology Process of Cyclopropyl-Z-phenylalanine methyl ester hydrochloride

There total 18 articles about Cyclopropyl-Z-phenylalanine methyl ester hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: methyl (1RS,2RS)-1-[(tert-butoxycarbonyl)amino]-2-phenyl-1-cyclopropanecarboxylate

: 82112-04-7,82112-05-8,110716-93-3,110716-94-4,121154-18-5,121154-19-6
Cyclopropyl-Z-phenylalanine methyl ester hydrochloride

Guidance literature:: With hydrogenchloride; In ethyl acetate; at 20 ℃; for 3h;
DOI:10.1016/j.bmc.2012.11.046

Reference yield:

: C₂₀H₂₁NO₃

: 82112-04-7,82112-05-8,110716-93-3,110716-94-4,121154-18-5,121154-19-6
methyl (E)-2-phenyl-1-aminocyclopropane-1-carboxylate hydrochloride

Guidance literature:: C₂₀H₂₁NO₃; With hydrogenchloride; In diethyl ether; at -20 ℃; for 0.333333h;

With hydrogenchloride; In diethyl ether; water; at -20 - 20 ℃;

Reference yield:

: 17606-70-1,5839-91-8
(4Z)-4-benzylidene-2-phenyl-1,3-oxazol-5(4H)-one

: 82112-04-7,82112-05-8,110716-93-3,110716-94-4,121154-18-5,121154-19-6
methyl (E)-2-phenyl-1-aminocyclopropane-1-carboxylate hydrochloride

Guidance literature:: Multi-step reaction with 4 steps

1: 100 percent / HBr (gas) / aq. HBr

2: 54 percent / CH₂Cl₂; diethyl ether / Ambient temperature

3: 97 percent / 4-(dimethylamino)pyridine / 0.5 h / Ambient temperature

4: 1.) triethyloxonium tetrafluoroborate, 2.) 1 N aq. HCl / 1.) CH₂Cl₂, reflux, overnight, 2.) ether, room temperature, 30 min

With hydrogenchloride; dmap; hydrogen bromide; triethyloxonium fluoroborate; In diethyl ether; dichloromethane; hydrogen bromide;
DOI:10.1021/jo00138a014