2,6-bis[zinc-15'-(3'',5''-di-tert-butylphenol)-3',7',13',17'-tetramethyl-2',8',12',18'-tetraethylporphin-5'-yl]-4-tert-buthylphenol

Base Information

• Chemical Name: 2,6-bis[zinc-15'-(3'',5''-di-tert-butylphenol)-3',7',13',17'-tetramethyl-2',8',12',18'-tetraethylporphin-5'-yl]-4-tert-buthylphenol
• CAS No.: 1151947-93-1
• Molecular Formula: C₁₀₂H₁₂₂N₈OZn₂
• Molecular Weight: 1606.92

Synonyms:

Chemical Property of 2,6-bis[zinc-15'-(3'',5''-di-tert-butylphenol)-3',7',13',17'-tetramethyl-2',8',12',18'-tetraethylporphin-5'-yl]-4-tert-buthylphenol

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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Useful:

Technology Process of 2,6-bis[zinc-15'-(3'',5''-di-tert-butylphenol)-3',7',13',17'-tetramethyl-2',8',12',18'-tetraethylporphin-5'-yl]-4-tert-buthylphenol

There total 1 articles about 2,6-bis[zinc-15'-(3'',5''-di-tert-butylphenol)-3',7',13',17'-tetramethyl-2',8',12',18'-tetraethylporphin-5'-yl]-4-tert-buthylphenol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

2,6-bis[15'-(3'',5''-di-tert-butylphenol)-3',7',13',17'-tetramethyl-2',8',12',18'-tetraethylporphin-5'-yl]-4-tert-buthylphenol + zinc diacetate (557-34-6) → 2,6-bis[zinc-15'-(3'',5''-di-tert-butylphenol)-3',7',13',17'-tetramethyl-2',8',12',18'-tetraethylporphin-5'-yl]-4-tert-buthylphenol (1151947-93-1)

Guidance literature:

In benzene; porphin dissolved in benzene; tenfold excess of Zn salt added; mixt. heated and boiled for 40-50 min; monitored by UV spectroscopy; cooled; extd. (H2O); benzene soln. evapd.;chromd. on silica gel (CHCl3 as eluent); isolated by pptn. from CHCl3; elem. anal.;

DOI:10.1134/S1070363208030250

upstream raw materials:

zinc diacetate

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