2-(3-Oxo-cyclohex-1-enylmethyl)-furan-3-carboxylic acid

Base Information

Chemical Name:2-(3-Oxo-cyclohex-1-enylmethyl)-furan-3-carboxylic acid
CAS No.:82207-07-6
Molecular Formula:C₁₂H₁₂O₄
Molecular Weight:220.225
Hs Code.:

Synonyms:

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Chemical Property of 2-(3-Oxo-cyclohex-1-enylmethyl)-furan-3-carboxylic acid

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Technology Process of 2-(3-Oxo-cyclohex-1-enylmethyl)-furan-3-carboxylic acid

There total 2 articles about 2-(3-Oxo-cyclohex-1-enylmethyl)-furan-3-carboxylic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 16807-60-6
3-methoxycyclohex-2-en-1-one

: C₆H₄O₃^(2-)

: 82207-07-6
2-(3-Oxo-cyclohex-1-enylmethyl)-furan-3-carboxylic acid

Guidance literature:: DOI:10.1246/cl.1982.441

Reference yield:

: 6947-94-0
2-methyl-3-furancarboxylic acid

: 16807-60-6
3-methoxycyclohex-2-en-1-one

: 82207-07-6
2-(3-Oxo-cyclohex-1-enylmethyl)-furan-3-carboxylic acid

Guidance literature:: With lithium diisopropyl amide; Multistep reaction; 1) THF, hexane, -78 deg C, 30 min, 2) THF, r.t., 1 h;

Reference yield:

: 82207-07-6
2-(3-Oxo-cyclohex-1-enylmethyl)-furan-3-carboxylic acid

: 1856-58-2,22415-07-2,58511-33-4,66964-61-2,72523-74-1,77480-20-7,77480-21-8,108667-51-2
(+/-)-dihydrocallitrisin

Guidance literature:: Multi-step reaction with 12 steps

2: 89 percent / 45 h / 0 °C

3: 88 percent / TsOH / benzene

4: 94 percent / NaBH₄, NaOH / bis-(2-methoxy-ethyl) ether; H₂O / 120 °C

5: 92 percent / pyridine / Ambient temperature

7: H₂ / 5percent Pd/C / ethyl acetate

8: 100 percent / NaBH₄ / methanol

9: TsOH / acetone

10: KOH / methanol

11: 90 percent / tetrahydrofuran; hexamethylphosphoric acid triamide

12: LDA

With pyridine; potassium hydroxide; sodium hydroxide; sodium tetrahydroborate; hydrogen; toluene-4-sulfonic acid; lithium diisopropyl amide; palladium on activated charcoal; In tetrahydrofuran; methanol; N,N,N,N,N,N-hexamethylphosphoric triamide; diethylene glycol dimethyl ether; water; ethyl acetate; acetone; benzene;
DOI:10.1246/cl.1982.441