2-Methylthio-4-nitrostilben

Base Information

• Chemical Name: 2-Methylthio-4-nitrostilben
• CAS No.: 35717-52-3
• Molecular Formula: C₁₅H₁₃NO₂S
• Molecular Weight: 271.34
• Mol file: 35717-52-3.mol

Synonyms:

Chemical Property of 2-Methylthio-4-nitrostilben

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2-Methylthio-4-nitrostilben

There total 2 articles about 2-Methylthio-4-nitrostilben which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

benzaldehyde (100-52-7) → 2-Methylthio-4-nitrostilben (35717-52-3)

Guidance literature:

Multi-step reaction with 2 steps

1: NaOH / dimethylformamide

2: dimethylsulfoxide / Heating

With sodium hydroxide; In dimethyl sulfoxide; N,N-dimethyl-formamide;

DOI:10.1021/jm00293a023

Reference yield:

1-Phenyl-2-(2-methylthio-4-nitrophenyl)-ethanol (35717-51-2) → 2-Methylthio-4-nitrostilben (35717-52-3)

Guidance literature:

In dimethyl sulfoxide; Heating;

DOI:10.1021/jm00293a023

Reference yield:

2-Methylthio-4-nitrostilben (35717-52-3) → 2-Methylthio-4-stilbenamin

Guidance literature:

With hydrazine hydrate; palladium on activated charcoal;

DOI:10.1021/jm00293a023

upstream raw materials:

1-Phenyl-2-(2-methylthio-4-nitrophenyl)-ethanol

benzaldehyde