C₂₇H₁₉N₃O

Base Information

• Chemical Name: C₂₇H₁₉N₃O
• CAS No.: 1609021-29-5
• Molecular Formula: C₂₇H₁₉N₃O
• Molecular Weight: 401.467
• Mol file: 1609021-29-5.mol

Synonyms:

Chemical Property of C₂₇H₁₉N₃O

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₂₇H₁₉N₃O

There total 5 articles about C₂₇H₁₉N₃O which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 38.0%

2-hydroxy-3-(diphenylhydroxymethyl)anthracene (1609021-27-3) → C27H19N3O (1609021-29-5)

Guidance literature:

With sodium azide; In water; acetonitrile; for 2h; Irradiation; Inert atmosphere;

DOI:10.1021/jo500290y

Reference yield:

benzophenone (119-61-9) → C27H19N3O (1609021-29-5)

Guidance literature:

Multi-step reaction with 2 steps

1.1: n-butyllithium / diethyl ether; hexane / 0.5 h / -15 - 20 °C / Inert atmosphere

1.2: -10 - 20 °C / Inert atmosphere

2.1: sodium azide / acetonitrile; water / 2 h / Irradiation; Inert atmosphere

With n-butyllithium; sodium azide; In diethyl ether; hexane; water; acetonitrile;

DOI:10.1021/jo500290y

Reference yield:

3-bromo-2-hydroxyanthraquinone (72668-05-4) → C27H19N3O (1609021-29-5)

Guidance literature:

Multi-step reaction with 3 steps

1.1: sodium tetrahydroborate; isopropyl alcohol / water / 0.25 h / Reflux

2.1: n-butyllithium / diethyl ether; hexane / 0.5 h / -15 - 20 °C / Inert atmosphere

2.2: -10 - 20 °C / Inert atmosphere

3.1: sodium azide / acetonitrile; water / 2 h / Irradiation; Inert atmosphere

With sodium tetrahydroborate; n-butyllithium; sodium azide; isopropyl alcohol; In diethyl ether; hexane; water; acetonitrile;

DOI:10.1021/jo500290y

upstream raw materials:

benzophenone

3-bromo-2-hydroxyanthraquinone

3-bromo-2-hydroxyanthracene

2-hydroxy-3-(diphenylhydroxymethyl)anthracene