C₅₄H₆₄N₄O₈

Base Information

Chemical Name:C₅₄H₆₄N₄O₈
CAS No.:1415034-10-4
Molecular Formula:C₅₄H₆₄N₄O₈
Molecular Weight:897.124
Hs Code.:

C<sub>54</sub>H<sub>64</sub>N<sub>4</sub>O<sub>8</sub>

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₅₄H₆₄N₄O₈

Chemical Property:

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Technology Process of C₅₄H₆₄N₄O₈

There total 6 articles about C₅₄H₆₄N₄O₈ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1239425-82-1
C₁₅H₂₁NO₄

: C₃₉H₄₅N₃O₅

: 1415034-10-4
C₅₄H₆₄N₄O₈

Guidance literature:: With 1-hydroxy-7-aza-benzotriazole; N-ethyl-N,N-diisopropylamine; ((3H-[1,2,3]triazolo[4,5-b]pyridin-3-yl)oxy)tri(pyrrolidin-1-yl)phosphonium hexafluorophosphate(V); In tetrahydrofuran; at 0 - 20 ℃; for 28h;
DOI:10.1021/jm301630s

Reference yield:

: 951637-18-6
(3S,4S)-tert-butyl 4-amino-3-hydroxy-5-phenylpentanoate

: 1415034-10-4
C₅₄H₆₄N₄O₈

Guidance literature:: Multi-step reaction with 3 steps

1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; 1-hydroxy-7-aza-benzotriazole; N-ethyl-N,N-diisopropylamine / dichloromethane / 20 °C / Cooling with ice

2: hydrogen; palladium on activated charcoal / ethyl acetate / 2 h / 760.05 Torr

3: 1-hydroxy-7-aza-benzotriazole; N-ethyl-N,N-diisopropylamine; ((3H-[1,2,3]triazolo[4,5-b]pyridin-3-yl)oxy)tri(pyrrolidin-1-yl)phosphonium hexafluorophosphate(V) / tetrahydrofuran / 28 h / 0 - 20 °C

With 1-hydroxy-7-aza-benzotriazole; palladium on activated charcoal; hydrogen; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; ((3H-[1,2,3]triazolo[4,5-b]pyridin-3-yl)oxy)tri(pyrrolidin-1-yl)phosphonium hexafluorophosphate(V); In tetrahydrofuran; dichloromethane; ethyl acetate;
DOI:10.1021/jm301630s

Reference yield:

: 1415033-99-6
C₄₇H₅₁N₃O₇

: 1415034-10-4
C₅₄H₆₄N₄O₈

Guidance literature:: Multi-step reaction with 2 steps

1: hydrogen; palladium on activated charcoal / ethyl acetate / 2 h / 760.05 Torr

2: 1-hydroxy-7-aza-benzotriazole; N-ethyl-N,N-diisopropylamine; ((3H-[1,2,3]triazolo[4,5-b]pyridin-3-yl)oxy)tri(pyrrolidin-1-yl)phosphonium hexafluorophosphate(V) / tetrahydrofuran / 28 h / 0 - 20 °C

With 1-hydroxy-7-aza-benzotriazole; palladium on activated charcoal; hydrogen; N-ethyl-N,N-diisopropylamine; ((3H-[1,2,3]triazolo[4,5-b]pyridin-3-yl)oxy)tri(pyrrolidin-1-yl)phosphonium hexafluorophosphate(V); In tetrahydrofuran; ethyl acetate;
DOI:10.1021/jm301630s