4-ethoxy-6-methoxysalicylaldehyde

Base Information

Chemical Name:4-ethoxy-6-methoxysalicylaldehyde
CAS No.:78347-30-5
Molecular Formula:C₁₀H₁₂O₄
Molecular Weight:196.203
Hs Code.:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-ethoxy-6-methoxysalicylaldehyde

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Technology Process of 4-ethoxy-6-methoxysalicylaldehyde

There total 2 articles about 4-ethoxy-6-methoxysalicylaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 12.0%

: 3519-76-4
2,4-dihydroxy-6-methoxybenzaldehyde

: 80-40-0
ethyl ester of p-toluenesulfonic acid

: 78347-30-5
4-ethoxy-6-methoxysalicylaldehyde

Guidance literature:: With potassium carbonate; In N,N-dimethyl-formamide; at 110 - 120 ℃; for 8h;
DOI:10.1007/BF00503335

Reference yield:

: 2174-64-3
5-methoxyresorcinol

: 78347-30-5
4-ethoxy-6-methoxysalicylaldehyde

Guidance literature:: Multi-step reaction with 2 steps

1: 69.4 percent / POCl₃ / diethyl ether / 1.)reflux, 1.5 h 2.)standing, 24 h

2: 12 percent / K₂CO₃ / dimethylformamide / 8 h / 110 - 120 °C

With potassium carbonate; trichlorophosphate; In diethyl ether; N,N-dimethyl-formamide;
DOI:10.1007/BF00503335