4-methylene-(amino)cyclooctane

Base Information

Chemical Name:4-methylene-(amino)cyclooctane
CAS No.:155127-64-3
Molecular Formula:C₁₇H₂₃NO₂
Molecular Weight:273.375
Hs Code.:

4-methylene-(<benzyloxycarbonyl>amino)cyclooctane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-methylene-(amino)cyclooctane

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Technology Process of 4-methylene-(amino)cyclooctane

There total 1 articles about 4-methylene-(amino)cyclooctane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 52.0%

: 1779-49-3
Methyltriphenylphosphonium bromide

: 155127-63-2
4-(amino)cyclooctanone

: 155127-64-3
4-methylene-(amino)cyclooctane

Guidance literature:: With sodium hydride; dimethyl sulfoxide; for 18h; Ambient temperature;
DOI:10.1016/S0040-4020(01)80257-X

Reference yield:

: 155127-64-3
4-methylene-(amino)cyclooctane

: N-(benzyloxycarbonyl)-1-methyl-9-azabicyclo<4.2.1>nonane

: N-(benzyloxycarbonyl)-1-hydroxymethyl-9-azabicyclo<4.2.1>nonane

Guidance literature:: With sodium tetrahydroborate; mercury(II) trifluoroacetate; Yield given. Multistep reaction. Yields of byproduct given; 1.) acetonitrile, 2.5 h, RT; 2.) THF, 3.5 h, RT;
DOI:10.1016/S0040-4020(01)80257-X