S-α,α-dimethylphenacyl thioacetate

Base Information

• Chemical Name: S-α,α-dimethylphenacyl thioacetate
• CAS No.: 14225-58-2
• Molecular Formula: C₁₂H₁₄O₂S
• Molecular Weight: 222.308
• Mol file: 14225-58-2.mol

Synonyms:

Chemical Property of S-α,α-dimethylphenacyl thioacetate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of S-α,α-dimethylphenacyl thioacetate

There total 3 articles about S-α,α-dimethylphenacyl thioacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

α-chloroisobutyrophenone (7473-99-6) → S-α,α-dimethylphenacyl thioacetate (14225-58-2)

Guidance literature:

Multi-step reaction with 2 steps

1: H₂S, NaOMe / methanol

2: Py

With pyridine; hydrogen sulfide; sodium methylate; In methanol;

DOI:10.1007/BF00902605

Reference yield:

2-isopropyl-5,5-dimethyl-2,4-diphenyl-2,5-dihydro-thiazole (14225-53-7) → S-α,α-dimethylphenacyl thioacetate (14225-58-2)

Guidance literature:

Multi-step reaction with 2 steps

1: aq. HCl / dioxane

2: Py

With pyridine; hydrogenchloride; In 1,4-dioxane;

DOI:10.1007/BF00902605

Reference yield:

α,α-dimethylphenacylthiol (14225-56-0) + acetic anhydride (108-24-7) → S-α,α-dimethylphenacyl thioacetate (14225-58-2)

Guidance literature:

With pyridine;

DOI:10.1007/BF00902605

upstream raw materials:

α,α-dimethylphenacylthiol

acetic anhydride

α-chloroisobutyrophenone

2-isopropyl-5,5-dimethyl-2,4-diphenyl-2,5-dihydro-thiazole