(+/-)-1-O-benzoyl-2,3-O-cyclohexylidene-4,5-O-isopropylidene-myo-inositol

Base Information

Chemical Name:(+/-)-1-O-benzoyl-2,3-O-cyclohexylidene-4,5-O-isopropylidene-myo-inositol
CAS No.:64290-81-9
Molecular Formula:C₂₂H₂₈O₇
Molecular Weight:404.46
Hs Code.:

Synonyms:

Suppliers and Price of (+/-)-1-O-benzoyl-2,3-O-cyclohexylidene-4,5-O-isopropylidene-myo-inositol

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of (+/-)-1-O-benzoyl-2,3-O-cyclohexylidene-4,5-O-isopropylidene-myo-inositol

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of (+/-)-1-O-benzoyl-2,3-O-cyclohexylidene-4,5-O-isopropylidene-myo-inositol

There total 1 articles about (+/-)-1-O-benzoyl-2,3-O-cyclohexylidene-4,5-O-isopropylidene-myo-inositol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 64290-81-9
C₂₂H₂₈O₇

Guidance literature:: Inosit 1c, 2,2-Dimethoxypropan, TsOH (neben Verb. 2f);
DOI:10.1246/bcsj.50.1867

Reference yield:

: 64290-81-9
(+/-)-1-O-benzoyl-2,3-O-cyclohexylidene-4,5-O-isopropylidene-myo-inositol

: 124516-85-4
(+/-)-6-O-benzyl-2,3-O-cyclohexylidene-1,4,5-tri-O-methoxymethyl-myo-inositol

Guidance literature:: Multi-step reaction with 4 steps

1: 1.) 50percent NaH, 2.) 1N KOH / 1.) DMF, mineral oil, 0 deg C, 30 min then R_.T_., 2 h, 2.) MeOH, R_.T_., 2 h

2: 89 percent / 50percent NaH / dimethylformamide; paraffin / 0 deg C, 30 min then R_.T_., 3 h

3: 92 percent / 1percent trifluoroacetic acid / CH₂Cl₂ / 0.5 h / Ambient temperature

4: 6 percent / 50percent NaH / dimethylformamide; paraffin / 0 deg C, 30 min then R_.T_., 2 h

With potassium hydroxide; sodium hydride; trifluoroacetic acid; In dichloromethane; N,N-dimethyl-formamide; paraffin;
DOI:10.1248/cpb.37.791

Reference yield:

: 64290-81-9
(+/-)-1-O-benzoyl-2,3-O-cyclohexylidene-4,5-O-isopropylidene-myo-inositol

: 124516-86-5,124580-63-8
C₃₄H₄₈O₁₅

Guidance literature:: Multi-step reaction with 5 steps

1: 1.) 50percent NaH, 2.) 1N KOH / 1.) DMF, mineral oil, 0 deg C, 30 min then R_.T_., 2 h, 2.) MeOH, R_.T_., 2 h

2: 89 percent / 50percent NaH / dimethylformamide; paraffin / 0 deg C, 30 min then R_.T_., 3 h

3: 92 percent / 1percent trifluoroacetic acid / CH₂Cl₂ / 0.5 h / Ambient temperature

4: 34.8 percent / 50percent NaH / dimethylformamide; paraffin / 0 deg C, 30 min then R_.T_., 2 h

5: 38.9 percent / silver triflate, 1,1,3,3-tetramethylurea / CH₂Cl₂ / 3 h / Ambient temperature; in the dark

With potassium hydroxide; silver trifluoromethanesulfonate; sodium hydride; trifluoroacetic acid; tetramethylurea; In dichloromethane; N,N-dimethyl-formamide; paraffin;
DOI:10.1248/cpb.37.791