dibenzyl (1S,2S)-1,2-dihydroxypropylphosphonate

Base Information

• Chemical Name: dibenzyl (1S,2S)-1,2-dihydroxypropylphosphonate
• CAS No.: 357174-85-7
• Molecular Formula: C₁₇H₂₁O₅P
• Molecular Weight: 336.324

Synonyms:

Chemical Property of dibenzyl (1S,2S)-1,2-dihydroxypropylphosphonate

Chemical Property:

Purity/Quality:

Safty Information:

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Technology Process of dibenzyl (1S,2S)-1,2-dihydroxypropylphosphonate

There total 1 articles about dibenzyl (1S,2S)-1,2-dihydroxypropylphosphonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

dibenzyl (E)-1-propenylphosphonate (159413-13-5) → dibenzyl (1S,2S)-1,2-dihydroxypropylphosphonate (357174-85-7) + dibenzyl (1R,2R)-1,2-dihydroxypropylphosphonate

Guidance literature:

With Hydroquinone 1,4-phthalazinediyl diether; potassium dioxotetrahydroxoosmate(VI); potassium hexacyanoferrate(III); potassium carbonate; In water; tert-butyl alcohol; at 0 ℃; for 144h; Further Variations:; Temperatures; reaction times; Product distribution;

DOI:10.1021/jo010701u

Reference yield: 49.0%

p-toluenesulfonyl chloride (98-59-9) + dibenzyl (1S,2S)-1,2-dihydroxypropylphosphonate (357174-85-7) → Toluene-4-sulfonic acid (1S,2S)-1-(bis-benzyloxy-phosphoryl)-2-hydroxy-propyl ester + C3H5PO3(C7H7)2H2O2(SO2C7H6)2

Guidance literature:

With triethylamine; In dichloromethane; at 5 ℃; for 53h; Further Variations:; Temperatures; reaction times; Product distribution;

DOI:10.1021/jo010701u

Reference yield:

4-Nitrobenzenesulfonyl chloride (98-74-8) + dibenzyl (1S,2S)-1,2-dihydroxypropylphosphonate (357174-85-7) → 4-Nitro-benzenesulfonic acid (1S,2S)-1-(bis-benzyloxy-phosphoryl)-2-hydroxy-propyl ester

Guidance literature:

With triethylamine; In dichloromethane; at 5 ℃; for 30h;

DOI:10.1021/jo010701u

upstream raw materials:

dibenzyl (E)-1-propenylphosphonate

Downstream raw materials:

dibenzyl (1R,2S)-1,2-epoxypropylphosphonate

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