2,3-Diamino-6-methylbenzoic acid

Base Information

Chemical Name:2,3-Diamino-6-methylbenzoic acid
CAS No.:124341-39-5
Molecular Formula:C₈H₁₀N₂O₂
Molecular Weight:166.18
Hs Code.:
DSSTox Substance ID:DTXSID101301731

Synonyms:2,3-diamino-6-methylbenzoic acid;124341-39-5;SCHEMBL7597578;RYTXFKCONVHCQC-UHFFFAOYSA-N;DTXSID101301731;1,2-diamino-4-methylcarboxybenzene

Suppliers and Price of 2,3-Diamino-6-methylbenzoic acid

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2,3-Diamino-6-methylbenzoic acid

Chemical Property:

XLogP3:1
Hydrogen Bond Donor Count:3
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:1
Exact Mass:166.074227566
Heavy Atom Count:12
Complexity:184

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CC1=C(C(=C(C=C1)N)N)C(=O)O

Technology Process of 2,3-Diamino-6-methylbenzoic acid

There total 5 articles about 2,3-Diamino-6-methylbenzoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 124341-09-9
5-bromo-6-methyl-3-nitroanthranilic acid

: 124341-39-5
2,3-diamino-6-methylbenzoic acid

Guidance literature:: With sodium hydroxide; hydrogen; palladium on activated charcoal;
DOI:10.1021/jm00164a054

Reference yield:

: 106976-22-1
5-bromo-4-methylisatin

: 124341-39-5
2,3-diamino-6-methylbenzoic acid

Guidance literature:: Multi-step reaction with 5 steps

1: 27percent H₂O₂, 3percent aq. NaOH

2: 70 percent / AcOH / 0.17 h / 90 - 95 °C

3: 68 percent / fuming HNO₃ / 0.17 h / 5 °C

4: 97 percent / aq. NaOH / 5 h / 90 °C

5: H₂, aq. NaOH / Pd/C

With sodium hydroxide; hydrogen; dihydrogen peroxide; nitric acid; acetic acid; palladium on activated charcoal;
DOI:10.1021/jm00164a054

Reference yield:

: 124341-06-6
6-amino-3-bromo-2-methylbenzoic acid

: 124341-39-5
2,3-diamino-6-methylbenzoic acid

Guidance literature:: Multi-step reaction with 4 steps

1: 70 percent / AcOH / 0.17 h / 90 - 95 °C

2: 68 percent / fuming HNO₃ / 0.17 h / 5 °C

3: 97 percent / aq. NaOH / 5 h / 90 °C

4: H₂, aq. NaOH / Pd/C

With sodium hydroxide; hydrogen; nitric acid; acetic acid; palladium on activated charcoal;
DOI:10.1021/jm00164a054