Technology Process of C12H15NO2
There total 5 articles about C12H15NO2 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 7 steps
1: magnesium / tetrahydrofuran / 20 °C
2: 3,3-dimethyldioxirane; sodium hydrogencarbonate / water; acetone / 20 °C
3: ethanol; sodium / tetrahydrofuran / 20 °C
4: sodium chloride / dimethyl sulfoxide / 150 °C
5: trimethylaluminum; ammonium chloride / toluene / 40 °C
6: sulfur trioxide pyridine complex; N-ethyl-N,N-diisopropylamine / dichloromethane; dimethyl sulfoxide / 150 °C
7: pyridinium p-toluenesulfonate / methanol / 20 °C
With
ethanol; trimethylaluminum; sodium; 3,3-dimethyldioxirane; sulfur trioxide pyridine complex; pyridinium p-toluenesulfonate; sodium hydrogencarbonate; ammonium chloride; magnesium; N-ethyl-N,N-diisopropylamine; sodium chloride;
In
tetrahydrofuran; methanol; dichloromethane; water; dimethyl sulfoxide; acetone; toluene;
DOI:10.1016/j.bmcl.2012.05.065
- Guidance literature:
-
Multi-step reaction with 2 steps
1: sulfur trioxide pyridine complex; N-ethyl-N,N-diisopropylamine / dichloromethane; dimethyl sulfoxide / 150 °C
2: pyridinium p-toluenesulfonate / methanol / 20 °C
With
sulfur trioxide pyridine complex; pyridinium p-toluenesulfonate; N-ethyl-N,N-diisopropylamine;
In
methanol; dichloromethane; dimethyl sulfoxide;
DOI:10.1016/j.bmcl.2012.05.065
