6-(4-hydroxy-3-methyl-2-butenyl)-2,3,5-trimethyl-1,4-benzoquinone

Base Information

Chemical Name:6-(4-hydroxy-3-methyl-2-butenyl)-2,3,5-trimethyl-1,4-benzoquinone
CAS No.:77879-10-8
Molecular Formula:C₁₄H₁₈O₃
Molecular Weight:234.295
Hs Code.:

Synonyms:

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Chemical Property of 6-(4-hydroxy-3-methyl-2-butenyl)-2,3,5-trimethyl-1,4-benzoquinone

Chemical Property:

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Technology Process of 6-(4-hydroxy-3-methyl-2-butenyl)-2,3,5-trimethyl-1,4-benzoquinone

There total 5 articles about 6-(4-hydroxy-3-methyl-2-butenyl)-2,3,5-trimethyl-1,4-benzoquinone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 700-13-0
Trimethylhydroquinone

: 77879-10-8
6-(4-hydroxy-3-methyl-2-butenyl)-2,3,5-trimethyl-1,4-benzoquinone

Guidance literature:: Multi-step reaction with 5 steps

1: 1.) BF₃/Et₂O, 2.) FeCl₃ / 1.) dioxane, RT, 90 min, 2.) dioxane/aq. methanol, RT, 10 min

2: 85 percent / Zn / pyridine / 0.5 h / Ambient temperature

3: 81 percent / OsO₄, NaIO₄ / dioxane; H₂O / 1 h / Ambient temperature

4: 92 percent / benzene / 1 h / Heating

5: 1.) NaAlH₂(OCH₂CH₂OCH₃)2, 2.) FeCl₃ / 1.) benzene, RT, 2 h, 2.) aq. MeOH, RT, 30 min

With sodium periodate; osmium(VIII) oxide; diethyl ether; boron trifluoride; iron(III) chloride; sodium bis(2-methoxyethoxy)aluminium dihydride; zinc; In 1,4-dioxane; pyridine; water; benzene;
DOI:10.1248/cpb.30.2797

Reference yield:

: 84978-30-3
2',5'-diacetoxy-3',4',6'-trimethylphenylacetaldehyde

: 77879-10-8
6-(4-hydroxy-3-methyl-2-butenyl)-2,3,5-trimethyl-1,4-benzoquinone

Guidance literature:: Multi-step reaction with 2 steps

1: 92 percent / benzene / 1 h / Heating

2: 1.) NaAlH₂(OCH₂CH₂OCH₃)2, 2.) FeCl₃ / 1.) benzene, RT, 2 h, 2.) aq. MeOH, RT, 30 min

With iron(III) chloride; sodium bis(2-methoxyethoxy)aluminium dihydride; In benzene;
DOI:10.1248/cpb.30.2797

Reference yield:

: 84978-28-9
2,3,5-trimethyl-6-(3-phenyl-2-propenyl)-1,4-benzoquinone

: 77879-10-8
6-(4-hydroxy-3-methyl-2-butenyl)-2,3,5-trimethyl-1,4-benzoquinone

Guidance literature:: Multi-step reaction with 4 steps

1: 85 percent / Zn / pyridine / 0.5 h / Ambient temperature

2: 81 percent / OsO₄, NaIO₄ / dioxane; H₂O / 1 h / Ambient temperature

3: 92 percent / benzene / 1 h / Heating

4: 1.) NaAlH₂(OCH₂CH₂OCH₃)2, 2.) FeCl₃ / 1.) benzene, RT, 2 h, 2.) aq. MeOH, RT, 30 min

With sodium periodate; osmium(VIII) oxide; iron(III) chloride; sodium bis(2-methoxyethoxy)aluminium dihydride; zinc; In 1,4-dioxane; pyridine; water; benzene;
DOI:10.1248/cpb.30.2797