N-{3-[N-Ethoxycarbonyl-N'-(4-nitro-benzoyl)-hydrazino]-2-oxo-cyclohexyl}-N'-(4-nitro-benzoyl)-hydrazinecarboxylic acid ethyl ester

Base Information

• Chemical Name: N-{3-[N-Ethoxycarbonyl-N'-(4-nitro-benzoyl)-hydrazino]-2-oxo-cyclohexyl}-N'-(4-nitro-benzoyl)-hydrazinecarboxylic acid ethyl ester
• CAS No.: 80330-96-7
• Molecular Formula: C₂₆H₂₈N₆O₁₁
• Molecular Weight: 600.542
• Mol file: 80330-96-7.mol

Synonyms:

Chemical Property of N-{3-[N-Ethoxycarbonyl-N'-(4-nitro-benzoyl)-hydrazino]-2-oxo-cyclohexyl}-N'-(4-nitro-benzoyl)-hydrazinecarboxylic acid ethyl ester

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of N-{3-[N-Ethoxycarbonyl-N'-(4-nitro-benzoyl)-hydrazino]-2-oxo-cyclohexyl}-N'-(4-nitro-benzoyl)-hydrazinecarboxylic acid ethyl ester

There total 4 articles about N-{3-[N-Ethoxycarbonyl-N'-(4-nitro-benzoyl)-hydrazino]-2-oxo-cyclohexyl}-N'-(4-nitro-benzoyl)-hydrazinecarboxylic acid ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

cyclohexanone (108-94-1,11119-77-0,9003-41-2,9075-99-4) → N-{3-[N-Ethoxycarbonyl-N'-(4-nitro-benzoyl)-hydrazino]-2-oxo-cyclohexyl}-N'-(4-nitro-benzoyl)-hydrazinecarboxylic acid ethyl ester (80330-96-7)

Guidance literature:

Multi-step reaction with 2 steps

1: p-toluenesulphonic acid / benzene / Heating

2: 2) HCl / 1) ether, 0 grad C,48 hr; 2) aceton, 2 day, room temperature

With hydrogenchloride; toluene-4-sulfonic acid; In benzene;

DOI:10.1016/S0040-4020(01)92366-X

Reference yield:

N-p-nitrobenzoyl-N'-ethoxycarbonyl hydrazine (23767-28-4) → N-{3-[N-Ethoxycarbonyl-N'-(4-nitro-benzoyl)-hydrazino]-2-oxo-cyclohexyl}-N'-(4-nitro-benzoyl)-hydrazinecarboxylic acid ethyl ester (80330-96-7)

Guidance literature:

Multi-step reaction with 2 steps

1: N-bromosuccinimide

2: 2) HCl / 1) ether, 0 grad C,48 hr; 2) aceton, 2 day, room temperature

With hydrogenchloride; N-Bromosuccinimide;

DOI:10.1016/S0040-4020(01)92366-X

Reference yield:

N-amino-(4-nitrophenyl)carboxamide (636-97-5) → N-{3-[N-Ethoxycarbonyl-N'-(4-nitro-benzoyl)-hydrazino]-2-oxo-cyclohexyl}-N'-(4-nitro-benzoyl)-hydrazinecarboxylic acid ethyl ester (80330-96-7)

Guidance literature:

Multi-step reaction with 3 steps

1: 66 percent

2: N-bromosuccinimide

3: 2) HCl / 1) ether, 0 grad C,48 hr; 2) aceton, 2 day, room temperature

With hydrogenchloride; N-Bromosuccinimide;

DOI:10.1016/S0040-4020(01)92366-X

upstream raw materials:

1-(1-Cyclohexen-1-yl)pyrrolidine

ethyl p-nitrobenzoylazocarboxylate

N-p-nitrobenzoyl-N'-ethoxycarbonyl hydrazine

cyclohexanone