4,4'-dideuteriohydrazobenzene

Base Information

• Chemical Name: 4,4'-dideuteriohydrazobenzene
• CAS No.: 95373-13-0
• Molecular Formula: C₁₂H₁₂N₂
• Molecular Weight: 186.225
• Mol file: 95373-13-0.mol

Synonyms:

Chemical Property of 4,4'-dideuteriohydrazobenzene

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 4,4'-dideuteriohydrazobenzene

There total 4 articles about 4,4'-dideuteriohydrazobenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4,4'-dideuterioazobenzene (35427-74-8) → 4,4'-dideuteriohydrazobenzene (95373-13-0)

Guidance literature:

With ammonium chloride; zinc;

DOI:10.1021/ja00394a047

Reference yield:

nitrobenzene-4-d (13122-36-6) → 4,4'-dideuteriohydrazobenzene (95373-13-0)

Guidance literature:

Multi-step reaction with 2 steps

2: zinc powder, NH₄Cl

With ammonium chloride; zinc;

DOI:10.1021/ja00394a047

Reference yield:

4-nitrobenzenediazonium tetrafluoroborate (456-27-9) → 4,4'-dideuteriohydrazobenzene (95373-13-0)

Guidance literature:

Multi-step reaction with 3 steps

1: D₃PO₄

3: zinc powder, NH₄Cl

With ammonium chloride; [D₃]phosphoric acid; zinc;

DOI:10.1021/ja00394a047

upstream raw materials:

4,4'-dideuterioazobenzene

nitrobenzene-4-d

4-nitrobenzenediazonium tetrafluoroborate