nitrobenzene-4-d

Base Information

• Chemical Name: nitrobenzene-4-d
• CAS No.: 13122-36-6
• Molecular Formula: C₆H₅NO₂
• Molecular Weight: 124.103
• Mol file: 13122-36-6.mol

Synonyms:nitrobenzene-4-d

Chemical Property of nitrobenzene-4-d

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

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Technology Process of nitrobenzene-4-d

There total 11 articles about nitrobenzene-4-d which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

para-nitrophenyl bromide (586-78-7) → nitrobenzene-4-d (13122-36-6)

Guidance literature:

With sodium formate; dimethyl sulfoxide; triphenylphosphine; bis(dibenzylideneacetone)-palladium⁽⁰⁾; at 80 ℃; for 8h; Inert atmosphere;

Reference yield: 88.0%

1-(methylsulfonyl)-2-(4-nitrophenyl)diazene (56075-39-9) → nitrobenzene-4-d (13122-36-6)

Guidance literature:

With 1,1,1,2,3,3,3-heptadeuterio-2-propanol; In water; for 14h; Reagent/catalyst; Irradiation;

DOI:10.3390/molecules24112164

Reference yield: 73.0%

4-nitrophenylhydrazone (100-16-3) → nitrobenzene-4-d (13122-36-6)

Guidance literature:

With ammonium cerium (IV) nitrate; d⁽⁴⁾-methanol; at 20 ℃;

DOI:10.1055/s-2007-1072749

upstream raw materials:

3,3-diethyl-1-(4-nitrophenyl)triaz-1-ene

4-nitrophenyl radical

4-nitrobenzenediazonium tetrafluoroborate

4-nitro-aniline

Downstream raw materials:

4,4'-dideuteriohydrazobenzene

4,4'-dideuteroazoxybenzene

4,4'-dideuterioazobenzene

4,4'-dideuterioazobenzene