O,O'-Di(tert-butyl)-N,N'-(propan-1,3-diyl)-N-<4-<<3-(tosylamino)propyl>amino>butyl>bis

Base Information

Chemical Name:O,O'-Di(tert-butyl)-N,N'-(propan-1,3-diyl)-N-<4-<<3-(tosylamino)propyl>amino>butyl>bis
CAS No.:134935-57-2
Molecular Formula:C₂₇H₄₈N₄O₆S
Molecular Weight:556.767
Hs Code.:

O,O'-Di(tert-butyl)-N,N'-(propan-1,3-diyl)-N-<4-<<3-(tosylamino)propyl>amino>butyl>bis<carbamat>

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Chemical Property of O,O'-Di(tert-butyl)-N,N'-(propan-1,3-diyl)-N-<4-<<3-(tosylamino)propyl>amino>butyl>bis

Chemical Property:

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Technology Process of O,O'-Di(tert-butyl)-N,N'-(propan-1,3-diyl)-N-<4-<<3-(tosylamino)propyl>amino>butyl>bis

There total 6 articles about O,O'-Di(tert-butyl)-N,N'-(propan-1,3-diyl)-N-<4-<<3-(tosylamino)propyl>amino>butyl>bis which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 107199-54-2
3-<(4-Hydroxybutyl)amino>propannitril

: 134935-57-2
O,O'-Di(tert-butyl)-N,N'-(propan-1,3-diyl)-N-<4-<<3-(tosylamino)propyl>amino>butyl>bis

Guidance literature:: Multi-step reaction with 4 steps

1: H₂, conc. HCl / PtO₂ / ethanol / 20 h / 22 °C / 2585.7 Torr

2: 95 percent / Na₂CO₃ / dioxane; H₂O / 1 h

3: 26 percent / oxalyl chloride / dimethylsulfoxide; CH₂Cl₂ / 0.5 h / -50 °C

4: 17 mg / 3-Angstroem molecular sieves, NaBH₄ / ethanol / 0.33 h / 0 °C

With hydrogenchloride; sodium tetrahydroborate; oxalyl dichloride; 3 A molecular sieve; hydrogen; sodium carbonate; platinum(IV) oxide; In 1,4-dioxane; ethanol; dichloromethane; water; dimethyl sulfoxide;
DOI:10.1002/hlca.19910740322

Reference yield:

: 56125-49-6
N-(3-aminopropyl)-p-toluenesulfonamide

: 134935-56-1
O,O'-Di(tert-butyl)-N-(3-formylpropyl)-N,N'-(propan-1,3-diyl)bis

: 134935-57-2
O,O'-Di(tert-butyl)-N,N'-(propan-1,3-diyl)-N-<4-<<3-(tosylamino)propyl>amino>butyl>bis

Guidance literature:: With sodium tetrahydroborate; 3 A molecular sieve; In ethanol; at 0 ℃; for 0.333333h;
DOI:10.1002/hlca.19910740322

Reference yield:

: 38353-77-4
N-(N³-p-toluenesulfonyl)-3-aminopropylphthalimide

: 134935-57-2
O,O'-Di(tert-butyl)-N,N'-(propan-1,3-diyl)-N-<4-<<3-(tosylamino)propyl>amino>butyl>bis

Guidance literature:: Multi-step reaction with 2 steps

1: 70 percent / N₂H₄*H₂O / ethanol / 1 h / Heating

2: 17 mg / 3-Angstroem molecular sieves, NaBH₄ / ethanol / 0.33 h / 0 °C

With sodium tetrahydroborate; 3 A molecular sieve; hydrazine hydrate; In ethanol;
DOI:10.1002/hlca.19910740322