C₁₈H₁₆BrClN₂O₂

Base Information

Chemical Name:C₁₈H₁₆BrClN₂O₂
CAS No.:1247090-75-0
Molecular Formula:C₁₈H₁₆BrClN₂O₂
Molecular Weight:407.694
Hs Code.:

C<sub>18</sub>H<sub>16</sub>BrClN<sub>2</sub>O<sub>2</sub>

Synonyms:

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Chemical Property of C₁₈H₁₆BrClN₂O₂

Chemical Property:

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Technology Process of C₁₈H₁₆BrClN₂O₂

There total 1 articles about C₁₈H₁₆BrClN₂O₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 67197-54-0
2-(4-bromo-2-chlorophenyl)acetonitrile

: 28447-17-8
3-(pyridin-3-yl)acrylic acid ethyl ester

: 1247090-75-0
C₁₈H₁₆BrClN₂O₂

Guidance literature:: With sodium ethanolate; In ethanol;
DOI:10.1016/j.bmcl.2012.01.044

Reference yield:

: 1247090-75-0
C₁₈H₁₆BrClN₂O₂

: C₃₇H₄₀ClN₃O₄

Guidance literature:: Multi-step reaction with 4 steps

1: sulfuric acid; acetic acid

2: dimethylsulfide borane complex / tetrahydrofuran

3: N-ethyl-N,N-diisopropylamine / dichloromethane

4: palladium diacetate; sodium carbonate; triphenylphosphine / propan-1-ol

With dimethylsulfide borane complex; sulfuric acid; palladium diacetate; sodium carbonate; acetic acid; N-ethyl-N,N-diisopropylamine; triphenylphosphine; In tetrahydrofuran; propan-1-ol; dichloromethane; 4: Suzuki coupling;
DOI:10.1016/j.bmcl.2012.01.044

Reference yield:

: 1247090-75-0
C₁₈H₁₆BrClN₂O₂

: C₂₉H₃₄ClN₃O₂

Guidance literature:: Multi-step reaction with 5 steps

1: sulfuric acid; acetic acid

2: dimethylsulfide borane complex / tetrahydrofuran

3: N-ethyl-N,N-diisopropylamine / dichloromethane

4: palladium diacetate; sodium carbonate; triphenylphosphine / propan-1-ol

5: palladium on activated charcoal; hydrogen / methanol

With dimethylsulfide borane complex; sulfuric acid; palladium on activated charcoal; hydrogen; palladium diacetate; sodium carbonate; acetic acid; N-ethyl-N,N-diisopropylamine; triphenylphosphine; In tetrahydrofuran; methanol; propan-1-ol; dichloromethane; 4: Suzuki coupling;
DOI:10.1016/j.bmcl.2012.01.044