2-methyl-4-trityl-aniline

Base Information

• Chemical Name: 2-methyl-4-trityl-aniline
• CAS No.: 101984-94-5
• Molecular Formula: C₂₆H₂₃N
• Molecular Weight: 349.475
• Mol file: 101984-94-5.mol

Synonyms:

Chemical Property of 2-methyl-4-trityl-aniline

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2-methyl-4-trityl-aniline

There total 12 articles about 2-methyl-4-trityl-aniline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

acetic acid-(2-methyl-4-trityl-anilide) (121791-90-0) → 2-methyl-4-trityl-aniline (101984-94-5)

Guidance literature:

With hydrogenchloride; ethanol;

DOI:10.1021/ja01855a077

Reference yield:

(4-amino-3-methylphenyl)(phenyl)methanone (4934-55-8) → 2-methyl-4-trityl-aniline (101984-94-5)

Guidance literature:

Multi-step reaction with 4 steps

1: diethyl ether / Erhitzen des nach dem Behandeln mit Wasser erhaltenen Reaktionsprodukts mit Acetanhydrid und Essigsaeure

2: acetic acid

3: sulfuric acid; pentyl nitrite; acetic acid / Erwaermen des Reaktionsprodukts mit Zink in Aethanol

4: hydrogen chloride; ethanol

With hydrogenchloride; diethyl ether; n-Amyl nitrite; ethanol; sulfuric acid; acetic acid;

DOI:10.1021/ja01855a077

Reference yield:

N-benzoyl-2-methylaniline (584-70-3) → 2-methyl-4-trityl-aniline (101984-94-5)

Guidance literature:

Multi-step reaction with 5 steps

1: zinc chloride / 220 °C

2: diethyl ether / Erhitzen des nach dem Behandeln mit Wasser erhaltenen Reaktionsprodukts mit Acetanhydrid und Essigsaeure

3: acetic acid

4: sulfuric acid; pentyl nitrite; acetic acid / Erwaermen des Reaktionsprodukts mit Zink in Aethanol

5: hydrogen chloride; ethanol

With hydrogenchloride; diethyl ether; n-Amyl nitrite; ethanol; sulfuric acid; acetic acid; zinc(II) chloride;

DOI:10.1021/ja01855a077

upstream raw materials:

triphenylmethyl alcohol

o-toluidine hydrochloride

N-trityl-o-toluidine

(E)-3-Ureido-but-2-enoic acid ethyl ester

Downstream raw materials:

1-Iodo-2-methyl-4-trityl-benzene

2-methyl-4-(2-methyl-4-trityl-phenyl)-but-3-yn-2-ol

o-methyl-p-tritylphenylacetylene

(3-methylphenyl)triphenylmethane